Citation: Jiali Lei, Juan Wang, Wenhui Zhang, Guohong Wang, Zihui Liang, Jinmao Li. TiO₂/CdIn₂S₄ S-scheme heterojunction photocatalyst promotes photocatalytic hydrogen evolution coupled vanillyl alcohol oxidation[J]. Acta Physico-Chimica Sinica, ;2025, 41(12): 100174. doi: 10.1016/j.actphy.2025.100174 shu

TiO₂/CdIn₂S₄ S-scheme heterojunction photocatalyst promotes photocatalytic hydrogen evolution coupled vanillyl alcohol oxidation

Jiali Lei ¹ ,
Juan Wang ^1,, ,
Wenhui Zhang ¹ ,
Guohong Wang ^1,, ,
Zihui Liang ² ,
Jinmao Li ^1,,

1.
Hubei Key Laboratory of Pollutant Analysis and Reuse Technology, College of Chemistry and Chemical Engineering, Hubei Normal University, Huangshi 435002, Hubei Province, China
2.
National Local Joint Laboratory for Advanced Textile Processing and Clean Production, Wuhan Textile University, Wuhan 430073, Hubei Province, China

Corresponding author: Juan Wang, wangjuan830508@163.com Guohong Wang, wanggh2003@163.com Jinmao Li, jemolee@126.com
Received Date: 26 July 2025
Revised Date: 24 August 2025
Accepted Date: 25 August 2025

Fund Project: the National Natural Science Foundation of China 52003079the National Natural Science Foundation of China 22075072Natural Science Foundation of Hubei Province 2023AFD027Natural Science Foundation of Hubei Province 2024AFB238Scientific Research Project of Education Department of Hubei Province D20232504the Open Research Fund of National Local Joint Laboratory for Advanced Textile Processing and Clean Production, Wuhan Textile University FX20240019

In this paper, a dual-function TiO₂/CdIn₂S₄ S-scheme heterojunction photocatalyst was fabricated through electrospinning and hydrothermal methods for hydrogen generation coupled with the selective oxidation of vanillyl alcohol (VAL) to vanillin (VN). The results indicate that the hybrid material containing 0.5 wt% CdIn₂S₄ possesses the best photocatalytic performance. The hydrogen generation rate reaches 403.36 μmol g⁻¹ h⁻¹. Meanwhile, the conversion of VAL is measured to be 90.99%. The results of experiments and density functional theory (DFT) calculations elucidate that the S-scheme heterojunction enhances the rate of charge migration and improves the efficiency of charge separation. In this system, the photoexcited holes with stronger oxidation capacity are reserved to catalyze the conversion of VAL into VN, while the photoexcited electrons with stronger reduction capacity are utilized to generate hydrogen. This study introduces a promising strategy that combines photocatalytic hydrogen generation with the selective conversion of organic compounds, offering novel insights into the development of innovative photocatalysts for effective solar energy utilization.
- TiO₂/CdIn₂S₄,
- S-scheme heterojunction,
- Dual-function photocatalyst,
- Vanillyl alcohol,
- Selective oxidation
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

TiO2/CdIn2S4 S-scheme heterojunction photocatalyst promotes photocatalytic hydrogen evolution coupled vanillyl alcohol oxidation

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通讯作者: 陈斌, bchen63@163.com

TiO₂/CdIn₂S₄ S-scheme heterojunction photocatalyst promotes photocatalytic hydrogen evolution coupled vanillyl alcohol oxidation