Citation: Shumin Zhang, Yaqi Wang, Zelin Wang, Libo Wang, Changsheng An, Difa Xu. Ultrafast electron transfer at the ZIS_1−x/UCN S-scheme interface enables efficient H₂O₂ photosynthesis coupled with tetracycline degradation[J]. Acta Physico-Chimica Sinica, ;2025, 41(11): 100136. doi: 10.1016/j.actphy.2025.100136 shu

Ultrafast electron transfer at the ZIS_1−x/UCN S-scheme interface enables efficient H₂O₂ photosynthesis coupled with tetracycline degradation

Shumin Zhang ¹ ,
Yaqi Wang ¹ ,
Zelin Wang ¹ ,
Libo Wang ² ,
Changsheng An ^1,, ,
Difa Xu ^1,,

1.
Hunan Key Laboratory of Applied Environmental Photocatalysis, Changsha University, Changsha 410022, Hunan Province, China
2.
Laboratory of Solar Fuel, Faculty of Materials Science and Chemistry, China University of Geosciences, Wuhan 430078, Hubei Province, China

Corresponding author: Changsheng An, z20190628@ccsu.edu.cn Difa Xu, xudifa@sina.com
Received Date: 24 June 2025
Revised Date: 20 July 2025
Accepted Date: 23 July 2025

Fund Project: the Research Foundation Bureau of Hunan Province 24B0787the National Natural Science Foundation of China 52204307the National Natural Science Foundation of China 52202376

Coupling H₂O₂ production with organic pollutant degradation can effectively overcome the sluggish kinetics of water oxidation while concurrently addressing environmental pollution challenges. In this work, an S-defect-rich ZnIn₂S₄/g-C₃N₄ (ZIS_1−x/UCN) S-scheme heterojunction photocatalyst was constructed by in situ growing ZIS_1−x nanosheets on porous ultrathin UCN. The designed ZIS_1−x/UCN photocatalyst demonstrates enhanced visible light absorption, abundant active sites, and intimate interfacial contact. The optimized ZIS_1−x/UCN-1.0 photocatalyst exhibits outstanding dual functionality, simultaneously achieving an H₂O₂ production rate of 2902.2 µmol·g⁻¹·h⁻¹ and 91.3% tetracycline (50 mg·L⁻¹) degradation efficiency. This H₂O₂ performance represents a 1.63-fold enhancement compared to its activity in pure water (1777.0 µmol·g⁻¹·h⁻¹). Through comprehensive characterization including femtosecond transient absorption spectroscopy (fs-TAS), in situ irradiation X-ray photoelectron spectroscopy (ISI-XPS), and in situ X-ray absorption fine structure spectroscopy (XAFS), we unequivocally confirm the S-scheme charge transfer mechanism. This S-scheme induced unique electronic structure not only fosters ultrafast electron transfer at the interface (3.54 ps) but also significantly enhances the redox capacity of photogenerated carriers. Collectively, this work opens new avenues for the dual application of photocatalytic technology in both energy production and environmental remediation.
- S-scheme heterojunction,
- H₂O₂ photosynthesis,
- Tetracycline degradation,
- fs-TA spectroscopy
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Ultrafast electron transfer at the ZIS1−x/UCN S-scheme interface enables efficient H2O2 photosynthesis coupled with tetracycline degradation

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通讯作者: 陈斌, bchen63@163.com

Ultrafast electron transfer at the ZIS_1−x/UCN S-scheme interface enables efficient H₂O₂ photosynthesis coupled with tetracycline degradation