Citation: Qinhui Guan, Yuhao Guo, Na Li, Jing Li, Tingjiang Yan. Molecular sieve-mediated indium oxide catalysts for enhancing photocatalytic CO₂ hydrogenation[J]. Acta Physico-Chimica Sinica, ;2025, 41(11): 100133. doi: 10.1016/j.actphy.2025.100133 shu

Molecular sieve-mediated indium oxide catalysts for enhancing photocatalytic CO₂ hydrogenation

Qinhui Guan ¹ ,
Yuhao Guo ¹ ,
Na Li ^2,, ,
Jing Li ³ ,
Tingjiang Yan ^{1, 2,,}

1.
College of Chemistry and Chemical Engineering, Shaanxi University of Science and Technology, Xi'an 710021, Shannxi Province, China
2.
School of Chemistry and Chemical Engineering, Qufu Normal University, Qufu 273165, Shandong Province, China
3.
Key Laboratory of Photochemical Conversion and Optoelectronic Materials, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190, China

Corresponding author: Na Li, lina20201130@163.com Tingjiang Yan, tingjiangn@163.com
Received Date: 16 June 2025
Revised Date: 18 July 2025
Accepted Date: 20 July 2025

Fund Project: the National Natural Science Foundation of China 22172086the National Natural Science Foundation of China 22105117the Taishan Scholars Program of Shandong Province tsqn202103064the Major Basic Research Project of Shandong Province ZR2021ZD06

In the realm of photocatalytic CO₂ hydrogenation, the adsorption-desorption behaviors and dynamics of photogenerated carriers are pivotal determinants of the kinetic processes and overall efficiency of photocatalytic reactions. Herein, 5A molecular sieve-functionalized In₂O₃ composites (denoted as IO@5A-xwt%) were fabricated through a facile impregnation-calcination method. Among them, the IO@5A-5wt% composite, with the optimized loading amount of 5A molecular sieves, showcases outstanding performance in photocatalytic conversion of CO₂ to CO, achieving a CO production rate of 2610.55 μmol·g⁻¹·h⁻¹, which is 19 times higher than that of pristine In₂O₃. Moreover, the IO@5A-5wt% composite maintains acceptable catalytic stability after a prolonged experiment lasting 45 h and total of 108 cycles. A comprehensive series of characterization techniques and performance evaluations reveal that the incorporation of 5A molecular sieves significantly modulates the adsorption-desorption behavior and hole dynamics during photocatalytic reactions. The multi-channel architecture of 5A molecular sieves, featuring suitable pore sizes, effectively enhances CO₂ adsorption. Meanwhile, the surface hydroxyl groups of 5A molecular sieves facilitate the transfer of photogenerated holes, thereby suppressing the recombination of photogenerated carriers. Additionally, the reaction product H₂O desorbs more readily from the catalyst surface. These synergistic effects collectively constitute the key mechanism underlying the enhanced photocatalytic performance of the IO@5A-5wt% composite.
- Molecular sieve,
- In₂O₃,
- Molecular-selective reservoir,
- Photocatalysis,
- CO₂ hydrogenation
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Molecular sieve-mediated indium oxide catalysts for enhancing photocatalytic CO2 hydrogenation

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通讯作者: 陈斌, bchen63@163.com

Molecular sieve-mediated indium oxide catalysts for enhancing photocatalytic CO₂ hydrogenation