Citation: Jingping Li, Suding Yan, Jiaxi Wu, Qiang Cheng, Kai Wang. Improving hydrogen peroxide photosynthesis over inorganic/organic S-scheme photocatalyst with LiFePO₄[J]. Acta Physico-Chimica Sinica, ;2025, 41(9): 100104. doi: 10.1016/j.actphy.2025.100104 shu

Improving hydrogen peroxide photosynthesis over inorganic/organic S-scheme photocatalyst with LiFePO₄

College of Urban and Environmental Sciences, Huangshi Key Laboratory of Prevention and Control of Soil Pollution, Hubei Normal University, Huangshi 435002, Hubei Province, China

Corresponding author: Suding Yan, yansd@hbnu.edu.cn Kai Wang, wangkai@hbnu.edu.cn
Received Date: 1 April 2025
Revised Date: 5 May 2025
Accepted Date: 11 May 2025

Fund Project: the National Natural Science Foundation of China 22378104Hubei Provincial Natural Science Foundation of China 2025AFA093Hubei Provincial Natural Science Foundation of China 2022CFB504Outstanding Youth Science and Technology Innovation Team in Hubei Province T2023021

With the rapid development of new energy industries, the utilization of waste batteries has attracted the attention of researchers. Developing a hydrogen peroxide photosynthesis system with battery recycling materials as photocatalysts presents a significant challenge. In this study, an ultrasonic self-assembly technique is employed to integrate LiFePO₄ (LFPO) nanoparticles, derived from spent batteries, with g-C₃N₄ (CN) nanosheets, thereby creating an inorganic/organic S-scheme photocatalyst for the production of H₂O₂. In situ analyses using X-ray photoelectron spectroscopy (XPS) and Kelvin probe force microscopy (KPFM) demonstrate that the interaction between LFPO and CN facilitates the development of an internal electric field (IEF), which in turn gives rise to a distinctive S-scheme charge transfer mechanism. Combining electron spin resonance spectroscopy, radical-trapping experiments, and in situ DRIFTS spectra, three pathways for H₂O₂ formation are identified. Benefited from enhanced carrier separation, strong redox power, and multichannel H₂O₂ formation, the optimal composite shows an impressive H₂O₂-production rate of 3.22 mol∙g⁻¹∙h⁻¹ under simulated solar irradiation. This research provides a potential method to investigate a sustainable H₂O₂ photosynthesis pathway by designing S-scheme heterojunctions from spent battery materials.
- Photocatalysis,
- H₂O₂ production,
- Inorganic/organic heterojunction,
- Battery-based catalyst,
- S-scheme mechanism
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沈阳化工大学材料科学与工程学院沈阳 110142

Improving hydrogen peroxide photosynthesis over inorganic/organic S-scheme photocatalyst with LiFePO4

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通讯作者: 陈斌, bchen63@163.com

Improving hydrogen peroxide photosynthesis over inorganic/organic S-scheme photocatalyst with LiFePO₄