Citation: Xianghai Song, Xiaoying Liu, Zhixiang Ren, Xiang Liu, Mei Wang, Yuanfeng Wu, Weiqiang Zhou, Zhi Zhu, Pengwei Huo. Insights into the greatly improved catalytic performance of N-doped BiOBr for CO₂ photoreduction[J]. Acta Physico-Chimica Sinica, ;2025, 41(6): 100055. doi: 10.1016/j.actphy.2025.100055 shu

Insights into the greatly improved catalytic performance of N-doped BiOBr for CO₂ photoreduction

1.
Institute of Green Chemistry and Chemical Technology, School of Chemistry and Chemical Engineering, Jiangsu University, Zhenjiang 212013, Jiangsu Province, China;
2.
Jiangsu Higher Vocational College Engineering Research Center of Green Energy and Low Carbon Materials, Zhenjiang College, Zhenjiang 212028, Jiangsu Province, China;
3.
School of Agricultural Engineering, Jiangsu University, Zhenjiang 212013, Jiangsu Province, China;
4.
School of Chemistry and Chemical Engineering, Henan Polytechnic University, Jiaozuo 454003, Henan Province, China;
5.
International Innovation Center for Forest Chemicals and Materials, Nanjing Forestry University, Nanjing 210037, Jiangsu Province, China

Received Date: 26 November 2024
Revised Date: 23 January 2025
Accepted Date: 23 January 2025

Fund Project: The project was supported by the National Natural Science Foundation of China (22108102, 22078131), the Fundamental Research Funds for the Universities of Henan Province (NSFRF240609), the GHfund B (202302026857), the Science and Technology Planning Social Development Project of Zhenjiang City (SH2023102), the International Innovation Center for Forest Chemicals and Materials of Nanjing Forestry.

Photocatalytic carbon dioxide (CO₂) reduction represents a hopeful approach to addressing global energy and environmental issues. The quest for catalysts that demonstrate both high activity and selectivity for CO₂ conversion has attracted significant attention. In this study, ultrathin N-doped BiOBr was synthesized using a simple straightforward method. Systematic experimental results indicated that N-doping reduced the thickness of the BiOBr nanosheets and increased their specific surface area. Moreover, the efficiency of photogenerated charge carrier migration and the CO₂ adsorption capacity were significantly enhanced, contributing to improved CO₂ photoreduction performance. Experimental results showed that the 2N-BiOBr exhibited the best catalytic performance, with a CO evolution rate of 18.28 μmol·g^-1·h^-1 and nearly 100% CO selectivity in water, which was three times higher than that of pure BiOBr. The potential photocatalytic mechanism was investigated using in situ FTIR analysis and DFT simulations. Mechanistic studies revealed that N atoms replaced O atoms as adsorption centers, enhancing the strong adsorption selectivity towards CO₂ over O―H in BiOBr and facilitating the formation of key reaction intermediates. This study provides new perspectives on the creation and development of effective photocatalytic materials, offering theoretical support for the application of photocatalytic technology in energy and environmental science.
- N-doping,
- CO₂ adsorption,
- Ultrathin BiOBr,
- Photocatalyst,
- CO₂ reduction
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Insights into the greatly improved catalytic performance of N-doped BiOBr for CO2 photoreduction

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通讯作者: 陈斌, bchen63@163.com

Insights into the greatly improved catalytic performance of N-doped BiOBr for CO₂ photoreduction