引用本文:
Qing Han Li, Zhi Gang Zhao. Microwave-assisted synthesis of new N4-[bi-(4-fluorophenyl)-methyl]-piperazine thiosemicarbazones under solvent-free conditions[J]. Chinese Chemical Letters,
2008, 19(9): 1035-1038.
doi:
10.1016/j.cclet.2008.06.018
Citation: Qing Han Li, Zhi Gang Zhao. Microwave-assisted synthesis of new N4-[bi-(4-fluorophenyl)-methyl]-piperazine thiosemicarbazones under solvent-free conditions[J]. Chinese Chemical Letters, 2008, 19(9): 1035-1038. doi: 10.1016/j.cclet.2008.06.018
Citation: Qing Han Li, Zhi Gang Zhao. Microwave-assisted synthesis of new N4-[bi-(4-fluorophenyl)-methyl]-piperazine thiosemicarbazones under solvent-free conditions[J]. Chinese Chemical Letters, 2008, 19(9): 1035-1038. doi: 10.1016/j.cclet.2008.06.018
Microwave-assisted synthesis of new N4-[bi-(4-fluorophenyl)-methyl]-piperazine thiosemicarbazones under solvent-free conditions
摘要:
Six new N4-[bi-(4-fluorophenyl)-methyl]-piperazine thiosemicarbazones 3a-f have been prepared starting from[bi-(4-fluor-ophenyl)-methyl]-piperazine in solvent-free condition under microwave irradiation with excellent yields. Their structures have been determined by elemental analysis, IR, MS and 1H NMR data.
English
Microwave-assisted synthesis of new N4-[bi-(4-fluorophenyl)-methyl]-piperazine thiosemicarbazones under solvent-free conditions
Abstract:
Six new N4-[bi-(4-fluorophenyl)-methyl]-piperazine thiosemicarbazones 3a-f have been prepared starting from[bi-(4-fluor-ophenyl)-methyl]-piperazine in solvent-free condition under microwave irradiation with excellent yields. Their structures have been determined by elemental analysis, IR, MS and 1H NMR data.
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