引用本文:
Sheng Hua Li, Si Ping Pang, Xiao Tong Li, Yong Zhong Yu, Xin Qi Zhao. Synthesis of new tetrazene (N-N=N-N)-linked bi (1,2,4-triazole)[J]. Chinese Chemical Letters,
2007, 18(10): 1176-1177.
doi:
10.1016/j.cclet.2007.08.018
Citation: Sheng Hua Li, Si Ping Pang, Xiao Tong Li, Yong Zhong Yu, Xin Qi Zhao. Synthesis of new tetrazene (N-N=N-N)-linked bi (1,2,4-triazole)[J]. Chinese Chemical Letters, 2007, 18(10): 1176-1177. doi: 10.1016/j.cclet.2007.08.018
Citation: Sheng Hua Li, Si Ping Pang, Xiao Tong Li, Yong Zhong Yu, Xin Qi Zhao. Synthesis of new tetrazene (N-N=N-N)-linked bi (1,2,4-triazole)[J]. Chinese Chemical Letters, 2007, 18(10): 1176-1177. doi: 10.1016/j.cclet.2007.08.018
Synthesis of new tetrazene (N-N=N-N)-linked bi (1,2,4-triazole)
摘要:
The reaction of 4-amino-1, 2, 4-triazole with sodium dichloroisocyanurate (SDCI) afforded new tetrazene(N-N=N-N)-linked bi(1, 2, 4-triazole) 2a in excellent yield. Increasing the molar ratio of SDCI to 4-amino-1, 2, 4-triazole, the chlorinated product 1, 5, 5'-trichloro-4, 4'-azo-1, 2, 4-triazole (2b) was formed. These new compounds have been characterized by MS, 1H NMR, 13C NMR, and elemental analysis.
English
Synthesis of new tetrazene (N-N=N-N)-linked bi (1,2,4-triazole)
Abstract:
The reaction of 4-amino-1, 2, 4-triazole with sodium dichloroisocyanurate (SDCI) afforded new tetrazene(N-N=N-N)-linked bi(1, 2, 4-triazole) 2a in excellent yield. Increasing the molar ratio of SDCI to 4-amino-1, 2, 4-triazole, the chlorinated product 1, 5, 5'-trichloro-4, 4'-azo-1, 2, 4-triazole (2b) was formed. These new compounds have been characterized by MS, 1H NMR, 13C NMR, and elemental analysis.
扫一扫看文章
计量
- PDF下载量: 2
- 文章访问数: 656
- HTML全文浏览量: 7
下载:
