引用本文:
Wei Yuan HUANG, Yuan XIE. The Reaction of Sodium Perfluoroalkanesulfinate with PCl3[J]. Chinese Chemical Letters,
1990, 1(1): 27-28.
Citation: Wei Yuan HUANG, Yuan XIE. The Reaction of Sodium Perfluoroalkanesulfinate with PCl3[J]. Chinese Chemical Letters, 1990, 1(1): 27-28.
Citation: Wei Yuan HUANG, Yuan XIE. The Reaction of Sodium Perfluoroalkanesulfinate with PCl3[J]. Chinese Chemical Letters, 1990, 1(1): 27-28.
The Reaction of Sodium Perfluoroalkanesulfinate with PCl3
摘要:
The reaction between sodium perfluoroalkanesulfinate(1)(Rf=a, Cl(CF2)4;b, Cl(CF2)6;c, Cl(CF2)8;d, n-C6F13;e, n-C8F17;f, H(CF2)4OCF2CF2)andphosphorus trichloride in acetonitrile at 0℃ resulted in the formation of anunstable intermediate, which was hydrolysed directly with aqueous sodium hydro-xide solution to give the corresponding perfluorocarboxylic acid in good yield.
English
The Reaction of Sodium Perfluoroalkanesulfinate with PCl3
Abstract:
The reaction between sodium perfluoroalkanesulfinate(1)(Rf=a, Cl(CF2)4;b, Cl(CF2)6;c, Cl(CF2)8;d, n-C6F13;e, n-C8F17;f, H(CF2)4OCF2CF2)andphosphorus trichloride in acetonitrile at 0℃ resulted in the formation of anunstable intermediate, which was hydrolysed directly with aqueous sodium hydro-xide solution to give the corresponding perfluorocarboxylic acid in good yield.
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