引用本文:
Qing Min WANG, Run Qiu HUANG, Zai Guo LI, Rut Lian SHAO. Synthesis of N-t-Butyl-N'-Aminocarbonyl-N-(Substituted) Benzoylhydrazine Containing α-Aminoalkylphosphonate Groups[J]. Chinese Chemical Letters,
2000, 11(5): 401-402.
Citation: Qing Min WANG, Run Qiu HUANG, Zai Guo LI, Rut Lian SHAO. Synthesis of N-t-Butyl-N'-Aminocarbonyl-N-(Substituted) Benzoylhydrazine Containing α-Aminoalkylphosphonate Groups[J]. Chinese Chemical Letters, 2000, 11(5): 401-402.
Citation: Qing Min WANG, Run Qiu HUANG, Zai Guo LI, Rut Lian SHAO. Synthesis of N-t-Butyl-N'-Aminocarbonyl-N-(Substituted) Benzoylhydrazine Containing α-Aminoalkylphosphonate Groups[J]. Chinese Chemical Letters, 2000, 11(5): 401-402.
Synthesis of N-t-Butyl-N'-Aminocarbonyl-N-(Substituted) Benzoylhydrazine Containing α-Aminoalkylphosphonate Groups
摘要:
A variety of novel N-t-butyl-N'-aminocarbonyl-N-(substituted)benzoylhydrazines containing α-aminoalkylphosphonate groups were synthesized by the addition of N-t-butyl-N-(substituted)benzoylhydrazines to α-isocyanatoalkylphosphonates, which were synthesized by the reaction of α-aminoalkylphosphonates with triphosgene in good yields. The structures of products including by-products were confirmed by 1H NMR, 31P NMR, IR, mass spectroscopy, and elemental analysis.
English
Synthesis of N-t-Butyl-N'-Aminocarbonyl-N-(Substituted) Benzoylhydrazine Containing α-Aminoalkylphosphonate Groups
Abstract:
A variety of novel N-t-butyl-N'-aminocarbonyl-N-(substituted)benzoylhydrazines containing α-aminoalkylphosphonate groups were synthesized by the addition of N-t-butyl-N-(substituted)benzoylhydrazines to α-isocyanatoalkylphosphonates, which were synthesized by the reaction of α-aminoalkylphosphonates with triphosgene in good yields. The structures of products including by-products were confirmed by 1H NMR, 31P NMR, IR, mass spectroscopy, and elemental analysis.
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Key words:
- Diacylhydrazines
- / α-aminoalkylphosphonates
- / triphosgene
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