引用本文:
李笃信, 薄改梅, 张艳春. 用常压乙炔法合成10-乙烯基吩噻嗪[J]. 应用化学,
1996, 13(3): 115-116.
Citation: Li Duxin, Bo Gaimei, Zhang Yanchun. Synthesis of 10-Vinylphenothiazine with Acetylene Under Ordinary Pressure[J]. Chinese Journal of Applied Chemistry, 1996, 13(3): 115-116.
Citation: Li Duxin, Bo Gaimei, Zhang Yanchun. Synthesis of 10-Vinylphenothiazine with Acetylene Under Ordinary Pressure[J]. Chinese Journal of Applied Chemistry, 1996, 13(3): 115-116.
用常压乙炔法合成10-乙烯基吩噻嗪
English
Synthesis of 10-Vinylphenothiazine with Acetylene Under Ordinary Pressure
Abstract:
A new synthetic method of 10-vinylphenothiazine with C2H2 under ordinary pressure was reported.A mixture of phenothiazine and KOH in DMSO was treated with C2H2 at 170℃ for 10 h to give 97% of yield.The reaction mechanism was explored preliminarily.
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Key words:
- vinylphenothiazine
- / synthesis
- / photoconductor
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