引用本文:
邓润华, 宓爱巧, 蒋耀忠. 微波快速烷基化合成α-氨基酸[J]. 应用化学,
1993, 10(5): 108-109.
Citation: Deng Runhua, Mi Aiqiao, Jiang Yaozhong. SYNTHESIS OF α-AMINO ACID VIA RAPID ALKYLATION UNDER MICROWAVE[J]. Chinese Journal of Applied Chemistry, 1993, 10(5): 108-109.
Citation: Deng Runhua, Mi Aiqiao, Jiang Yaozhong. SYNTHESIS OF α-AMINO ACID VIA RAPID ALKYLATION UNDER MICROWAVE[J]. Chinese Journal of Applied Chemistry, 1993, 10(5): 108-109.
微波快速烷基化合成α-氨基酸
English
SYNTHESIS OF α-AMINO ACID VIA RAPID ALKYLATION UNDER MICROWAVE
Abstract:
Five α-amino acids were prepared by rapid alkylation without solvent under microwave and phase transfer catalysis. The alkylation lasted only for 1~2min. The α-amino acids were obtained by after hydrolysis. The overall yields were 43.6%~62.5%.
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Key words:
- N-benzylidene glycinate
- / amino acid
- / synthesis microwave
- / phase transfer catalysis
- / alkylation
- / hydrolysis
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