引用本文:
李笃信, 陈亮, 高晓燕. 四苯基卟啉制法的改进[J]. 应用化学,
1993, 10(5): 95-96.
Citation: Li Duxin, Chen Liang, Gao Xiaoyan. AN IMPROVED METHOD FOR PREPARATION OF TETRAPHENYLPORPHYRIN[J]. Chinese Journal of Applied Chemistry, 1993, 10(5): 95-96.
Citation: Li Duxin, Chen Liang, Gao Xiaoyan. AN IMPROVED METHOD FOR PREPARATION OF TETRAPHENYLPORPHYRIN[J]. Chinese Journal of Applied Chemistry, 1993, 10(5): 95-96.
四苯基卟啉制法的改进
English
AN IMPROVED METHOD FOR PREPARATION OF TETRAPHENYLPORPHYRIN
Abstract:
The method of preparation of tetraphenylporphyrin (H2TPP) has been improved by using a mixed solvent based on the propionic acid and thionyl chloride as oxidizing agent instead of 2, 3-dichloro-5,6-dicyanobenzoqinone. The yield of the pure H2TPP achieved 38%. Six complexes of H2TPP with Cu, Co, Ni, Fe, In, and La were prepared respectively.
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Key words:
- tetraphenylporphyrin
- / porphyrin metal complex
- / preparation
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