引用本文:
周晓霜, 刘菁, 徐杰, 谭忠印. 过氧甲酸水溶液氧化环戊烯制备戊二醛[J]. 应用化学,
2003, 20(6): 600-602.
Citation: ZHOU Xiao-Shuang, LIU Jing, XU Jie, TAN Zhong-Yin. Synthesis of Glutaraldehyde by Oxidation of Cyclopentene with Peroxyformic Acid[J]. Chinese Journal of Applied Chemistry, 2003, 20(6): 600-602.
Citation: ZHOU Xiao-Shuang, LIU Jing, XU Jie, TAN Zhong-Yin. Synthesis of Glutaraldehyde by Oxidation of Cyclopentene with Peroxyformic Acid[J]. Chinese Journal of Applied Chemistry, 2003, 20(6): 600-602.
过氧甲酸水溶液氧化环戊烯制备戊二醛
English
Synthesis of Glutaraldehyde by Oxidation of Cyclopentene with Peroxyformic Acid
Abstract:
A preparation method of glutaraldehyde by one-step oxidation of cyclopentene with peroxyformic acid is reported.The preparation is carried out in a mild reaction condition,time saving and without catalyst.The product is identified by MS and IR measurements.The results showed that the highest yield of glutaraldehyde 56.7% is obtained at optimum molar ratio of n(hydrogen peroxide):n(cyclopentene):n(formic acid)=1:3:3,reaction temperature 35℃ and reaction time 1 h.
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Key words:
- glutaraldehyde
- / cyclopentene
- / formic acid
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