引用本文:
王璠, 陈金龙, 陈群, 何明阳, 张卫红. 4-(4-溴丁基)苯乙烯的合成[J]. 应用化学,
2005, 22(8): 912-914.
Citation: WANG Fan, CHEN Jin-Long, CHEN Qun, HE Ming-Yang, ZHANG Wei-Hong. Synthesis of 4-(4-Bromobutyl) styrene[J]. Chinese Journal of Applied Chemistry, 2005, 22(8): 912-914.
Citation: WANG Fan, CHEN Jin-Long, CHEN Qun, HE Ming-Yang, ZHANG Wei-Hong. Synthesis of 4-(4-Bromobutyl) styrene[J]. Chinese Journal of Applied Chemistry, 2005, 22(8): 912-914.
4-(4-溴丁基)苯乙烯的合成
English
Synthesis of 4-(4-Bromobutyl) styrene
Abstract:
4-(4-Bromobutyl) styrene was synthesized from p-chloroacetophenone.p-Chloroacetophenone was hydrogenized with potassium hydrogenborane to obtain p-chlorophenylethanol,which was then dehydrated to yield p-chlorostyrene in the presence of potassium bisulfate,and finally p-chlorostyrene was reacted with magnesium to get Grignard reagent,which was then reacted with 1,4-dibromobutane to synthesize 4-(4-bromobutyl) styrene.MS,1H NMR and FT-IR were used to characterize the product.The results are consistent with the structure of 4-(4-bromobutyl) styrene.
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Key words:
- bromobutylstyrene
- / p-chloroacetophenone
- / p-chlorostyrene
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