基于二羟基萘二磺酸根的配合物Na3[Na5(dhns)2]·(phen)4·2H2O的合成、晶体结构和热稳定性

魏赞斌 解庆范 陈延民

引用本文: 魏赞斌, 解庆范, 陈延民. 基于二羟基萘二磺酸根的配合物Na3[Na5(dhns)2]·(phen)4·2H2O的合成、晶体结构和热稳定性[J]. 无机化学学报, 2013, 29(7): 1414-1418. doi: 10.3969/j.issn.1001-4861.2013.00.212 shu
Citation:  WEI Zan-Bin, XIE Qing-Fan, CHEN Yan-Min. Synthesis, Crystal Structure and Thermal Stability of Complex Na3[Na5(dhns)2]·(phen)4·2H2O with Bihydroxynaphthalenedisulfonate[J]. Chinese Journal of Inorganic Chemistry, 2013, 29(7): 1414-1418. doi: 10.3969/j.issn.1001-4861.2013.00.212 shu

基于二羟基萘二磺酸根的配合物Na3[Na5(dhns)2]·(phen)4·2H2O的合成、晶体结构和热稳定性

  • 基金项目:

    福建省教育厅科技基金(No.JA08212) (No.JA08212)

    福建省科技厅科技项目(No.2008F5053)资助项目。 (No.2008F5053)

摘要: 2,7-二羟基萘-3,6-二磺酸二钠盐(Na2H2dhns)与邻菲罗啉在乙醇/水溶液中自组装得到一新的配合物Na3[Na5(dhns)2]·(phen)4·2H2O (1),并用CHN元素分析、IR、TGA和X-射线单晶衍射分析进行了表征。晶体属正交晶系,Pna21空间群,a=2.829 85(12) nm,b=1.038 99(14) nm,c=2.259 23(13) nm,V=6.642 6(10) nm3,Z=4,Dc=1.573 g·cm-3,R1=0.050 6,wR2=0.124 0,S=1.05。

English

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  • 收稿日期:  2012-09-09
  • 网络出版日期:  2013-02-03
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