引用本文:
Azharullah Khan, Mahboob Alam, M. Mushfiq. The synthesis of 2'-amino-5α-cholest-6-eno [6,7-d]-thiazole derivatives under microwave irradiation using dry-media conditions[J]. Chinese Chemical Letters,
2008, 19(9): 1027-1030.
doi:
10.1016/j.cclet.2008.06.021
Citation: Azharullah Khan, Mahboob Alam, M. Mushfiq. The synthesis of 2'-amino-5α-cholest-6-eno [6,7-d]-thiazole derivatives under microwave irradiation using dry-media conditions[J]. Chinese Chemical Letters, 2008, 19(9): 1027-1030. doi: 10.1016/j.cclet.2008.06.021
Citation: Azharullah Khan, Mahboob Alam, M. Mushfiq. The synthesis of 2'-amino-5α-cholest-6-eno [6,7-d]-thiazole derivatives under microwave irradiation using dry-media conditions[J]. Chinese Chemical Letters, 2008, 19(9): 1027-1030. doi: 10.1016/j.cclet.2008.06.021
The synthesis of 2'-amino-5α-cholest-6-eno [6,7-d]-thiazole derivatives under microwave irradiation using dry-media conditions
摘要:
A convenient, rapid and efficient method for the synthesis of substituted steroidal[6,7-d] thiazoles using microwave-induced organic reaction enhancement chemistry has been developed. The additional features of this methodology include a much faster reaction, easy workup, high yield, high purity of the products and an environment friendly approach.
English
The synthesis of 2'-amino-5α-cholest-6-eno [6,7-d]-thiazole derivatives under microwave irradiation using dry-media conditions
Abstract:
A convenient, rapid and efficient method for the synthesis of substituted steroidal[6,7-d] thiazoles using microwave-induced organic reaction enhancement chemistry has been developed. The additional features of this methodology include a much faster reaction, easy workup, high yield, high purity of the products and an environment friendly approach.
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Key words:
- Dry media
- / Neutral alumina
- / Phenylthiourea
- / Iodine and saturated steroidal ketones
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