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温和条件下混合碱辅助水热合成硅酸镁纳米管

陈兰花 ,  李轩 ,  郭向可 ,  郭学锋 ,  丁维平

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引用本文: 陈兰花, 李轩, 郭向可, 郭学锋, 丁维平. 温和条件下混合碱辅助水热合成硅酸镁纳米管[J]. 无机化学学报, 2013, 29(7): 1333-1338. doi: 10.3969/j.issn.1001-4861.2013.00.277 shu
Citation:  CHEN Lan-Hua, LI Xuan, GUO Xiang-Ke, GUO Xue-Feng, DING Wei-Ping. Composite-Hydroxide-Assisted Hydrothermal Synthesis of Magnesium Silicate Nanotube[J]. Chinese Journal of Inorganic Chemistry, 2013, 29(7): 1333-1338. doi: 10.3969/j.issn.1001-4861.2013.00.277 shu

温和条件下混合碱辅助水热合成硅酸镁纳米管

  • 基金项目:

    国家重点基础研究项目(No.2009CB623504) (No.2009CB623504)

    国家科学自然基金(No.20773062,20773063,21173119,21273109)资助项目。 (No.20773062,20773063,21173119,21273109)

摘要: 在混和碱的辅助下,以普通氢氧化镁和二氧化硅粉末为原料在温和条件下高效合成硅酸镁纳米管。采用XRD,TEM,FTIR,氮气吸附等多种手段对产物进行了表征,并对其合成过程进行了研究。结果表明氢氧化钠和氢氧化钾的共融液能提高反应物间的溶解性,促进反应可以在温和条件下加快进行。250 ℃下合成硅酸镁纳米管,传统水热法至少需要7 d,混合辅助水热合成只需36 h。与传统的水热法相比,混和碱辅助的水热法是一种温和且高效的过程。

English

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  • 收稿日期:  2013-05-03
  • 网络出版日期:  2013-05-29
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