引用本文:
刘小兰, 孙命, 缪方明, 李玉桂, 王建基, 韩玉真, 徐筱杰. 1-氧代 -4-(取代)-2,6,7-三氧杂-1-磷杂双环[2,2,2]辛烷晶体结构研究[J]. 物理化学学报,
1992, 8(01): 100-108.
doi:
10.3866/PKU.WHXB19920118
Citation: Liu Xiao-Lan, Sun Ming, Miao Fang-Ming, Li Yu-Gui, Wang Jian-Ji, Han Yu-Zhen, Xu Xiao-Jie. Crystal and Molecular Structure of 1-Oxo-4-(Substituent)-1-Phospha-2,6,7-Trioxacyclo(2,2,2) Octane[J]. Acta Physico-Chimica Sinica, 1992, 8(01): 100-108. doi: 10.3866/PKU.WHXB19920118
Citation: Liu Xiao-Lan, Sun Ming, Miao Fang-Ming, Li Yu-Gui, Wang Jian-Ji, Han Yu-Zhen, Xu Xiao-Jie. Crystal and Molecular Structure of 1-Oxo-4-(Substituent)-1-Phospha-2,6,7-Trioxacyclo(2,2,2) Octane[J]. Acta Physico-Chimica Sinica, 1992, 8(01): 100-108. doi: 10.3866/PKU.WHXB19920118
1-氧代 -4-(取代)-2,6,7-三氧杂-1-磷杂双环[2,2,2]辛烷晶体结构研究
English
Crystal and Molecular Structure of 1-Oxo-4-(Substituent)-1-Phospha-2,6,7-Trioxacyclo(2,2,2) Octane
Abstract:
The crystal structure of four 1-oxo-4-(substituent)-1-phospha-2,6,7-trioxacyclo(2,2,2) octane have been determinded by dimention single-crystal X-ray analysis.
All intensity data were collected with an Enraf-Nonius CAD4 diffractometer, using graphite monochromated Cu-K_α radiation and ω/2θ scan, and corrected for LP and emperical absorption factors. All crystal structures were solved by MULTAN and refined by full matrix least-squares with lsotropic thermal vibration factors for H and anisotropic for the others.
Crystal data, (I) X=NH, R=H, ...
All intensity data were collected with an Enraf-Nonius CAD4 diffractometer, using graphite monochromated Cu-K_α radiation and ω/2θ scan, and corrected for LP and emperical absorption factors. All crystal structures were solved by MULTAN and refined by full matrix least-squares with lsotropic thermal vibration factors for H and anisotropic for the others.
Crystal data, (I) X=NH, R=H, ...
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