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Ag/ZIF-90自组装薄膜的制备及SERS活性研究

郑龙珍 ,  亢晓卫 ,  纪忆 ,  邹志君 ,  王益民 ,  陈计芳

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引用本文: 郑龙珍, 亢晓卫, 纪忆, 邹志君, 王益民, 陈计芳. Ag/ZIF-90自组装薄膜的制备及SERS活性研究[J]. 无机化学学报, 2015, (3): 465-471. doi: 10.11862/CJIC.2015.079 shu
Citation:  ZHENG Long-Zhen, KANG Xiao-Wei, JI Yi, ZOU Zhi-Jun, WANG Yi-Min, CHEN Ji-Fang. Preparation of Ag/ZIF-90 Self-Assembled Membrane and Its High SERS Performance[J]. Chinese Journal of Inorganic Chemistry, 2015, (3): 465-471. doi: 10.11862/CJIC.2015.079 shu

Ag/ZIF-90自组装薄膜的制备及SERS活性研究

  • 1.

    华东交通大学理学院, 南昌 330013

    • 通讯作者: 郑龙珍 zhenglongzhen@tsinghua.org.cn
  • 基金项目:

    国家自然科学基金(No.21163007, 21165009, 21465011) (No.21163007, 21165009, 21465011)

    江西省主要学科学术和技术带头人计划(No.20133BCB22007) (No.20133BCB22007)

    江西省自然科学 基金(No.20132BAB203012)资助项目。 (No.20132BAB203012)

摘要: 合成了金属有机框架化合物沸石咪唑框架-90(ZIF-90)溶胶和ZIF-90晶体薄膜, 分别以这2种材料为基底, 制备出了Ag@ZIF-90复合材料和Ag/ZIF-90自组装薄膜。通过傅里叶变换红外(FT-IR), X射线衍射(XRD), 扫描电子显微镜(SEM)对产物进行表征, 分析了它们的形貌和结构特征。以罗丹明6G(R 6G)作为检测分子, 对所制备材料的表面增强拉曼散射(SERS)性能进行测试。结果表明制备出的Ag/ZIF-90自组装薄膜具有好的SERS性能, 而ZIF-90本身的拉曼峰并不会对Ag/ZIF-90自组装薄膜对目标分子的SERS检测效果产生影响。这种材料可以作为一种良好的SERS检测基底, 在农药残留检测方面具有很好的应用前景。

English

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  • 收稿日期:  2014-08-16
  • 网络出版日期:  2014-11-07
通讯作者: 陈斌, bchen63@163.com
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