引用本文:
Barahman Movassagh, Amir Rakhshani. A mild and highly efficient one-pot three-component reaction for carbon-sulfur bond formation catalyzed by potassium tert-butoxide[J]. Chinese Chemical Letters,
2011, 22(10): 1179-1182.
doi:
10.1016/j.cclet.2011.05.015
Citation: Barahman Movassagh, Amir Rakhshani. A mild and highly efficient one-pot three-component reaction for carbon-sulfur bond formation catalyzed by potassium tert-butoxide[J]. Chinese Chemical Letters, 2011, 22(10): 1179-1182. doi: 10.1016/j.cclet.2011.05.015
Citation: Barahman Movassagh, Amir Rakhshani. A mild and highly efficient one-pot three-component reaction for carbon-sulfur bond formation catalyzed by potassium tert-butoxide[J]. Chinese Chemical Letters, 2011, 22(10): 1179-1182. doi: 10.1016/j.cclet.2011.05.015
A mild and highly efficient one-pot three-component reaction for carbon-sulfur bond formation catalyzed by potassium tert-butoxide
摘要:
Potassium tert-butoxide has been found to be a highly efficient catalyst for one-pot, three-component reaction of aryl aldehydes, acetophenones, and thiols via Claisen-Schmidt/Michael addition reactions for the synthesis of thia-Michael adducts in high yields. The reactions are best carried out in tert-butyl alcohol at room temperature.
English
A mild and highly efficient one-pot three-component reaction for carbon-sulfur bond formation catalyzed by potassium tert-butoxide
Abstract:
Potassium tert-butoxide has been found to be a highly efficient catalyst for one-pot, three-component reaction of aryl aldehydes, acetophenones, and thiols via Claisen-Schmidt/Michael addition reactions for the synthesis of thia-Michael adducts in high yields. The reactions are best carried out in tert-butyl alcohol at room temperature.
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Key words:
- Potassium tert-butoxide
- / Thia-Michael adduct
- / Three-component reaction
- / C-S bond formation
- / Thiols
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