引用本文:
Qian Rong LI, Sha YANG. Synthesis of A Novel Fulleroaziridine Carrying 4-Deoxy-4'-demethylepipodophyllotoxin[J]. Chinese Chemical Letters,
2003, 14(11): 1123-1126.
Citation: Qian Rong LI, Sha YANG. Synthesis of A Novel Fulleroaziridine Carrying 4-Deoxy-4'-demethylepipodophyllotoxin[J]. Chinese Chemical Letters, 2003, 14(11): 1123-1126.
Citation: Qian Rong LI, Sha YANG. Synthesis of A Novel Fulleroaziridine Carrying 4-Deoxy-4'-demethylepipodophyllotoxin[J]. Chinese Chemical Letters, 2003, 14(11): 1123-1126.
Synthesis of A Novel Fulleroaziridine Carrying 4-Deoxy-4'-demethylepipodophyllotoxin
摘要:
A novel fulleroaziridine 2 with a closed 6,6-ring junction was synthesized from[60]fullerene and 4-azido-4-deoxy-4'-demethylepipodophyllotoxin 1 in 1, 2-dichlorobenzene at 110℃ for 45 h, in a yield of 39.3% based on consumed C60. The structure of the product was characterized by NMR and MS.
English
Synthesis of A Novel Fulleroaziridine Carrying 4-Deoxy-4'-demethylepipodophyllotoxin
Abstract:
A novel fulleroaziridine 2 with a closed 6,6-ring junction was synthesized from[60]fullerene and 4-azido-4-deoxy-4'-demethylepipodophyllotoxin 1 in 1, 2-dichlorobenzene at 110℃ for 45 h, in a yield of 39.3% based on consumed C60. The structure of the product was characterized by NMR and MS.
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Key words:
- Podophyllotoxin derivative
- / azide
- / [60]fullerene
- / fulleroaziridine
- / cycloaddition
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