引用本文:
Yan He HUANG, De Quan YU. Total Synthesis of dl-Ligustiphenol[J]. Chinese Chemical Letters,
1996, 7(10): 896-897.
Citation: Yan He HUANG, De Quan YU. Total Synthesis of dl-Ligustiphenol[J]. Chinese Chemical Letters, 1996, 7(10): 896-897.
Citation: Yan He HUANG, De Quan YU. Total Synthesis of dl-Ligustiphenol[J]. Chinese Chemical Letters, 1996, 7(10): 896-897.
Total Synthesis of dl-Ligustiphenol
摘要:
—(-)S-Ligustiphenol is a new sesquiterpene compound with antiinflammatory and immunosuppressive activities.The total synthesis of its racemate was carried out by a six-step reaction sequence including bromination of aldehyde, iodination of m-cresol, protection of phenolic hydroxyl, Grignard reaction, aldol condensation, etc.The target compound was characterized by comparing its 1H NMR, MS and IR spectra with natural (-) ligustiphenol.
English
Total Synthesis of dl-Ligustiphenol
Abstract:
—(-)S-Ligustiphenol is a new sesquiterpene compound with antiinflammatory and immunosuppressive activities.The total synthesis of its racemate was carried out by a six-step reaction sequence including bromination of aldehyde, iodination of m-cresol, protection of phenolic hydroxyl, Grignard reaction, aldol condensation, etc.The target compound was characterized by comparing its 1H NMR, MS and IR spectra with natural (-) ligustiphenol.
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