引用本文:
Guo Ping XUE, Sheng Hua LIU, En Qin FU, Han Sheng XU, Cheng Tai WU. A CONVENIENT SYNTHESIS OF NEW HYDROXYL CYCLIC AZA COMPOUNDS[J]. Chinese Chemical Letters,
1994, 5(6): 457-458.
Citation: Guo Ping XUE, Sheng Hua LIU, En Qin FU, Han Sheng XU, Cheng Tai WU. A CONVENIENT SYNTHESIS OF NEW HYDROXYL CYCLIC AZA COMPOUNDS[J]. Chinese Chemical Letters, 1994, 5(6): 457-458.
Citation: Guo Ping XUE, Sheng Hua LIU, En Qin FU, Han Sheng XU, Cheng Tai WU. A CONVENIENT SYNTHESIS OF NEW HYDROXYL CYCLIC AZA COMPOUNDS[J]. Chinese Chemical Letters, 1994, 5(6): 457-458.
A CONVENIENT SYNTHESIS OF NEW HYDROXYL CYCLIC AZA COMPOUNDS
摘要:
A convenient synthetic route to a series of hydroxyl cyclic di-and tri-aza compounds was described.Condensation of 1,3-dichloropropanol[2] with the appropriate disodium salts of N-tosylated di-and triamine in EtOH gave the corresponding 7-,8-and 10-membered di-and triamine cycles in reasonable yields.The tosyl groups were removed with 33% HBr-HOAc in ca. 90% yields.
English
A CONVENIENT SYNTHESIS OF NEW HYDROXYL CYCLIC AZA COMPOUNDS
Abstract:
A convenient synthetic route to a series of hydroxyl cyclic di-and tri-aza compounds was described.Condensation of 1,3-dichloropropanol[2] with the appropriate disodium salts of N-tosylated di-and triamine in EtOH gave the corresponding 7-,8-and 10-membered di-and triamine cycles in reasonable yields.The tosyl groups were removed with 33% HBr-HOAc in ca. 90% yields.
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