Citation: Zheng LI, Xi Cun WANG. One-pot Synthesis of 1-Aryloxyacety l-4-(4'-nitrophenyloxyacetyl)-thiosemicarbazides under Phase Transfer Catalysis and Microwave Irradiation[J]. Chinese Chemical Letters, ;2002, 13(8): 717-720. shu

One-pot Synthesis of 1-Aryloxyacety l-4-(4'-nitrophenyloxyacetyl)-thiosemicarbazides under Phase Transfer Catalysis and Microwave Irradiation

Zheng LI ,
Xi Cun WANG

College of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou 730070

Received Date: 9 November 2001

Fund Project: The authors are grateful for financial support for this work from Scientific and Technological Innovation Engineering of Northwest Normal University (NWNU-KJCXGC-218), Natural Science Foundation of Gansu Province and Youth Foundation of Northwest Normal University.

The 1-aryloxyacetyl-4-(4'-nitrophenyloxyacetyl)-thiosemicarbazides (3a-h) are synthe-sized via reaction of 4-nitrophenyloxyacetyl chloride with ammonium thiocyanate and aryloxyacetic hydrazides (2a-h) under phase transfer catalysis and microwave irradiation in excellent yield.
- 1,4-Diaryloxyacetyl thiosemicarbazide,
- phase transfer catalysis,
- microwave irradiation
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