引用本文:
戴金水. 用八羰基合二钴在相转移催化条件下合成1-萘乙酸[J]. 应用化学,
1998, 15(1): 86-88.
Citation: Dai Jinshui. Phase-transfer-catalytic Synthesis of 1-Naphthalene Acetic Acid by Octacarbonyl Dicobalt[J]. Chinese Journal of Applied Chemistry, 1998, 15(1): 86-88.
Citation: Dai Jinshui. Phase-transfer-catalytic Synthesis of 1-Naphthalene Acetic Acid by Octacarbonyl Dicobalt[J]. Chinese Journal of Applied Chemistry, 1998, 15(1): 86-88.
用八羰基合二钴在相转移催化条件下合成1-萘乙酸
English
Phase-transfer-catalytic Synthesis of 1-Naphthalene Acetic Acid by Octacarbonyl Dicobalt
Abstract:
1-Naphthalene acetic acid was synthesized from 1-chloromethyl naphthalene by octacarbonyl dicobalt under phase transfer catalytic conditions. Conversion was 99% and yield 83%. The effects of reaction temperatures, ratios of reactants, solvents, contents of catalyst and concentration of alkali on conversion have been investigated. Among the phase transfer catalysts tested, the most effective was hexadecyltrimethylammonium chloride.
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