Citation: JI Jie, LI Hui, WANG Jia-ni, SUO Zhi, XU Ying. Effect of compatibilizer on low-temperature performances of modified asphalts from direct coal liquefaction residue[J]. Journal of Fuel Chemistry and Technology, ;2019, 47(8): 925-933. shu

Effect of compatibilizer on low-temperature performances of modified asphalts from direct coal liquefaction residue

JI Jie ^1,2,, ,
LI Hui ¹ ,
WANG Jia-ni ^1,2 ,
SUO Zhi ^1,2 ,
XU Ying ^1,2

1.
School of Civil Engineering and Transportation, Beijing University of Civil Engineering and Architecture, Beijing 100044, China
2.
Beijing Advanced Innovation Center for Future Urban Design, Beijing 100044, China

Corresponding author: JI Jie, jijie@bucea.edu.cn
Received Date: 8 April 2019
Revised Date: 5 June 2019

Fund Project: The project was supported by the National Natural Science Foundation of China(51778038), Beijing Natural Science Foundation Committee-Beijing Municipal Education Commission(KZ201910016017), Yangtse Rive Scholar and Innovation Team Development Plan(IRT-17R06), Fundamental Research Business Expenses of Municipal Universities-ZC Major Key Scientific Research Support Projects-ZC05 Scientific Research and Innovation Team Building Plan(X18259)Fundamental Research Business Expenses of Municipal Universities-ZC Major Key Scientific Research Support Projects-ZC05 Scientific Research and Innovation Team Building Plan X18259Yangtse Rive Scholar and Innovation Team Development Plan IRT-17R06Beijing Natural Science Foundation Committee-Beijing Municipal Education Commission KZ201910016017the National Natural Science Foundation of China 51778038

Figures(9)

In order to evaluate influence of different compatibilizers on low-temperature performances of direct coal liquefaction residue modified asphalts (DCLR modified asphalt), 3 compatibilizers including silane coupling agent, benzaldehyde and xylene were used. At first, the optimum dosage and mixing mode of the compatibilizers were determined by orthogonal test. Secondly, resistance to low-temperature cracking of the asphalt after adding compatibilizer was evaluated using the Double-Edge-Notched Tension (DENT) test. Finally, dispersion state of DCLR in asphalt were analyzed by scanning electron microscopy and software of Image Pro Plus diagram to quantitatively analyze low-temperature performances of the asphalts after adding compatibilizer. The test results show that addition of compatibilizer is helpful to improve dispersion of DCLR in asphalt and compatibility between them. Thus, the long-term stability of DCLR modified asphalt after adding compatibilizer can be maintained and its low-temperature performances are enhanced. Additionally, the 3 compatibilizers have different effects on low-temperature performances of the DCLR modified asphalt, silane coupling agent is the best, followed by benzaldehyde and xylene.
- compatibilizer,
- direct coal liquefaction residue modified asphalt,
- double edge notched tension test,
- low-temperature performance,
- dispersion area ratio
1. [1]
  ELLIOT M A. Chemistry of Coal Utilization (Second Supplementary Volume)[M]. New York:John Wiley and Sons, Inc, 1981.
2. [2]
  ZHENG L Z, WANG X H, ZHANG T S, ZHENG C H. Research progress in utilizations of coal liquefaction residues[C]//IEEE. 2011 International Conference on Materials for Renewable Energy and Environment. New York: IEEE. 2011: 1627-1630.
3. [3]
  PATEL P. China and south africa pursue coal liquefaction[J]. MRS Bulletin, 2012,37(3):204-205. doi: 10.1557/mrs.2012.64
4. [4]
  CN: 201010614927. (LAI Shi-liu, CHEN Xue-lian, SHENG Ying. An ionic liquid extractant used to separate asphaltenes, asphaltenes and heavy oils from direct coal liquefaction residue[P]. CN: 201010614927.
5. [5]
  ADACHI Y, NAKAMIZ M. Chemical structure of pyridine soluble matter of coal liquefaction residue[J]. J Japan Inst Energy, 1993,72(10):930-934. doi: 10.3775/jie.72.930
6. [6]
  SUGANO M, IKEMIZU R, MASHIMO K. Effects of the oxidation pretreatment with hydrogen peroxide on the hydrogenolysis reactivity of the coal liquefaction residue[J]. Fuel Process Technol, 2002,77/78(1):67-73.
7. [7]
  RATHBONE R F, HOWER J C, DERBYSHIRE F J. The application of fluorescence microscopy to coal-derived characterization[J]. Fuel, 1993,72(8):1177-1185. doi: 10.1016/0016-2361(93)90328-Y
8. [8]
  WANG Zhai-xia, YANG Jian-li, LIU Zhen-yu. Preliminary evaluation of direct coal liquefaction residue modification effect on road asphalt[J]. J Fuel Chem Technol, 2007,35(1):109-112. doi: 10.3969/j.issn.0253-2409.2007.01.021
9. [9]
  JI J, ZHAO Y S, XU S F. Study on properties of the Blends with Direct Coal Liquefaction Residue and Asphalt[C]//Materials Science, Civil Engineering and Architecture Science, Mechanical Engineering and Manufacturing Technology, ICAEMAS 2014. Xi'an, China, 2014. USA: Trans Tech Publication Inc, 2014: 316-321.
10. [10]
  JI Jie, SHI Yue-feng, SUO Zhi, XU Shi-fa, YANG Song, LI Peng-fei. Comparison on properties of modified asphalt blended with DCLR and TLA[J]. J Fuel Chem Technol, 2015,43(9):1061-1067. doi: 10.3969/j.issn.0253-2409.2015.09.006
11. [11]
  JI J, YAO H, YANG X, XU Y, SUO Z, YOU Z P. Performance analysis of direct coal liquefaction residue (DCLR) and Trinidad lake asphalt (TLA) for the purpose of modifying tradition alasphalt[J]. Arabian J Sci Engineer, 2016,41(10):3983-3993. doi: 10.1007/s13369-016-2034-5
12. [12]
  HE Liang. Research on preparation and properties of direct coal liquefaction residue modified asphalt[D]. Xi'an: Chang'an University, 2013.
13. [13]
  SU Man-man, ZHANG Hong-liang, ZHANG Yong-ping, ZHANG Zeng-ping. Miscibility and mechniclanical properties of SBS and asphalt blends based on molecular dynamics simulation[J]. J Chang'an Univ (Nat Sci Ed), 2017,37(3):24-32. doi: 10.3969/j.issn.1671-8879.2017.03.004
14. [14]
  LIU Ke-fei, DENG Lin-fei, ZHENG Jia-yu, JIANG Kang. Compatibility evaluation of waste tire rubber power modified asphalt binder[J]. New Build Mater, 2017,44(5):13-16. doi: 10.3969/j.issn.1001-702X.2017.05.004
15. [15]
  LI Kuan, PAN Yong-qiang, ZHANG Hui, CHEN Li-feng, ZHANG Jian. Research progress of compatibility of epoxy asphalt for steel deck pvement[J]. Mater Rev, 2018,32(9):1534-1540.
16. [16]
  CHEN Jing, SUN Ming, DAI Xiao-min, YAO Yi, LIU Yuan-yuan, HE Min, LÜ Bo, ZHAO Xiang-long, MA Xiao-xun. Asphalt modification with direct coal liquefaction residue based on benzaldehyde crosslinking agent[J]. J Fuel Chem Technol, 2015,43(9):1052-1060. doi: 10.3969/j.issn.0253-2409.2015.09.005
17. [17]
  CHAO Wei-dong, LIU Shu-tang. Effect of silane coupling agent on properties of asphalt-rubber(AR)binders[J]. J Build Mater, 2009,12(4):497-500. doi: 10.3969/j.issn.1007-9629.2009.04.026
18. [18]
  SU Da-gen, ZHANG Jing-feng, HE Juan. Study on the function of emulsified asphalt modified by silance coupling[J]. Guangzhou Chem Ind, 2006(3):32-34. doi: 10.3969/j.issn.1001-9677.2006.03.014
19. [19]
  FAN Yun-zhu. Exploratory study on properties and application of coal direct liquefaction residue[D]. Shanghai: East China University of Science and Technology, 2011.
20. [20]
  CHEN Song, PEI Xiao-guang, LIU Rong-bo. Evaluation method of low temperature performance of SBS modified asphalt[J]. Shandong Chem Ind, 2018,47(9):49-50+52. doi: 10.3969/j.issn.1008-021X.2018.09.020
21. [21]
  COTTERELL B, REDDEL J K. The essential work of plane stress ductile fracture[J]. Inter J Fract, 1977,13(3):267-277.
22. [22]
  ANDRIESCU A, HESP S, YOUTCHEFF J S. Essential and Plastic Works of Ductile Fracture in Asphalt Binders[M]. 2004.
23. [23]
  ZHOU F, MOGAWER W, LI H, ANDRIESCU A, COPELAND A. Evaluation of fatigue tests for characterizing asphalt binders[J]. J Mater Civ Eng, 2013,25(5):610-617. doi: 10.1061/(ASCE)MT.1943-5533.0000625
24. [24]
  TABATABAEE H, CLOPOTEL C, ARSHADI A. Critical problems with using the asphalt ductility test as a performance index for modified binders[J]. Transportation Research Record:Journal of the Transportation Research Board, 2013(2370):84-91.
25. [25]
  PALIUKAITE M, ASSURAS M, SILVA S C, DING H, GOTAME Y, NIE Y, UBAID I, HESP S A M. Implementation of the double-edge-notched tension test for asphalt cement acceptance[J]. Trans Dev Eco, 2017,3(1)6. doi: 10.1007/s40890-017-0034-0
26. [26]
  PALIUKAITE M, ASSURAS M, HESP S A M. Effect of recycled engine oil bottoms on the ductile failure properties ofstraight and polymer-modified asphalt cements[J]. Constr Build Mater, 2016,126:190-196. doi: 10.1016/j.conbuildmat.2016.08.156
27. [27]
  SINGH D, GIRIMATH S. Influence of RAP sources and proportions on fracture and low temperature cracking performance of polymer modified binder[J]. Constr Build Mater, 2016,120:10-18. doi: 10.1016/j.conbuildmat.2016.05.094
28. [28]
  AASHTO TP 113-15, Standard Method of Test for Determination of Asphalt Binder Resistance to Ductile Failure Using Double-Edge-Notched Tension (DENT) Test[S]. Washington, 2015.
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