Citation: Zheng Mingtao, Lu Qiming, Lei Bingfu, Dong Hanwu, Yang Lemin, Liu Yingliang. Preparation, Characterization and Hydrogen Storage Properties of Sulfur Doped Carbon Nanospheres——Exploration and Practice of Comprehensive Designing Experiment Teaching in Chemistry and Materials Related Disciplines[J]. Chemistry, ;2018, 81(6): 562-570. shu

Preparation, Characterization and Hydrogen Storage Properties of Sulfur Doped Carbon Nanospheres——Exploration and Practice of Comprehensive Designing Experiment Teaching in Chemistry and Materials Related Disciplines

College of Materials and Energy, South China Agricultural University, Guangzhou 510642

Received Date: 25 January 2018
Accepted Date: 28 March 2018

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Comprehensive designing experiment is one of the most important means for educating comprehensive quality and innovation ability of college students. This paper presents a comprehensive designing experiment of 'Preparation, characterization and hydrogen storage properties of sulfur doped carbon nanospheres'. Through the literature investigate and survey, experimental principle description, scheme establishment, sample preparation, structure characterization, performance evaluation, and data processing, the students can acquire the key knowledge of nanomaterials synthesis, component and structure characterization, property analysis, and so on. In addition, they can also get the development of comprehensive capability and innovation ability. Practice demonstrates that this comprehensive designing experiment can be beneficial to improve the practical capability, innovation ability, basic scientific literacy and comprehensive quality for college students.
- Sulfur doping,
- Carbon nanospheres,
- Comprehensive designing experiment,
- Innovation capability
1. [1]
2. [2]
3. [3]
4. [4]
5. [5]
  M Zheng, Y Liu, K Jiang et al. Carbon, 2010, 48:1224-1233.
6. [6]
  Y Zhong, X Xia, F Shi et al. Adv. Sci., 2016, 3:1500286.
7. [7]
  M Zheng, Y Xiao, H Zhang et al. Chin. J. Inorg. Chem., 2013, 29(7):1391-1399.
8. [8]
  M Zheng, Y Liu, Y Xiao et al. J. Phys. Chem. C, 2009, 113:8455-8459.
9. [9]
  Y E Gorbaty, R B Gupta. Ind. Eng. Chem. Res., 1998, 37(8):3026-3035.
10. [10]
  N Tsuchiya, Y Suto, T Kabuta et al. J. Mater. Sci., 2008, 43(7):2115-2122.
11. [11]
12. [12]
  M Zheng, Y Liu, Y Xiao et al. J. Phys. Chem. C, 2009, 113:8455-8459.
13. [13]
  H Feng, M Zheng, H Dong et al. J. Mater. Chem. A, 2015, 3, 15225-15234.
14. [14]
  G Compagnini, O Puglisi, G Foti. Carbon, 1997, 35(12):1793-1797.
15. [15]
  H Chadli, A Rahmani, K Sbai et al. Physica A, 2005, 358(1):226-236.
16. [16]
  L Tapasztó, K Kertész, Z Vértesy et al. Carbon, 2005, 43:970-977.
17. [17]
  P Tan, S Dimovski, Y Gogotsi. Phys. Eng. Sci., 2004, 362(1824):2289-2310.
18. [18]
  A M Puziy, O I Poddubnaya, R P Socha et al. Carbon, 2008, 46:2113-2123.
19. [19]
20. [20]
1. [1]
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2. [2]
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3. [3]
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