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Citation: QIAO Qing-Dong, LI Qi, YU Da-Yong, LIANG Hong-Yu. Preparation and Application of Ti-Supported Lead Dioxide Electrode[J]. Chinese Journal of Applied Chemistry, ;2000, 17(5): 555-557. shu

Preparation and Application of Ti-Supported Lead Dioxide Electrode

1.
Department of Applied Chemistry, Fushun Petroleum Institute, Fushun 113001

Received Date: 15 December 1999
Available Online: 6 May 2000
Fund Project: 辽宁省自然科学基金资助项目(962029) (962029)

The Ti-supported lead dioxide electrode(Ti/PdO₂) consisted of a Sb₂O₃/SnO₂ semiconductive interlayer and electrodeposited PbO₂ films was prepared. The optimum ratio of Sb₂O₃ to SnO₂ was 15%~25%. Addition of NaF(0.40 g/L) in electroplating solution could decrease the rate of PbO₂ deposition, which resulted in the formation of small crystal particles and compact PbO₂ films. XRD study showed the U-form crystal of electrode. The electrode was tested in synthesis of 4-picoline acid by electro-oxidation of 4-picoline, showing good electroconductivity and stable life.
- titanium based lead dioxide electrode,
- preparation,
- electro-oxidation reacted,
- picoline
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