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Citation: CHANG Huai-Chun, YANG Chang-Chun, WANG Xiu-Mei, WANG Hong-Bo, TONG Jian, SU Chang-An, GUO Wen-Sheng, CAI Yun-Ping, MA Ming-Yang, CHENG Guang-Rong, LÜ Yang. Isolation of Anisole from Volatile Oil of Foemiculum Vulgare Mill by Crystalline Inclusion Method[J]. Chinese Journal of Applied Chemistry, ;2001, 18(6): 440-443. shu

Isolation of Anisole from Volatile Oil of Foemiculum Vulgare Mill by Crystalline Inclusion Method

1.
a College of Chemical Science and Engineering, Liaoning University, Shenyang 110036;
2.
b Institute of Applied Chemistry, Liaoning University, Shenyang 110036;
3.
c Liaoning Provincial Center of Analysis, Testing and Research, Shenyang;
4.
d Medicine Institute, Chinese Academy of Medical Science, Beijing

Received Date: 27 October 2000
Available Online: 8 January 2001
Fund Project: 国家自然科学基金资助项目(29875035) (29875035)

The chemical components of volatile oil from Foemiculum Vulgare Mill were determined by GC-MS, amomg them 82.65% were anisole. A selective isolation of anisole from the volatile oil from mentioned seed has been carried out by an inclusion method. 1,1,6,6-Tetraphenyl-hexa-2,4-diyne-1,6-diol(abbrv. DD) was used as a host molecule with anisole being as a guest molecule. The structure of the inclusion complex was characterized by IR, XRD, ¹H NMR techniques and the host-guest molar ratio in complex was found to be 3:1. The anisole was isolated from inclusion complex by using Kugelrohr vacuum distillation technique and the isolated compound was characterized to be trans-anisole.
- anisole,
- volatile oil,
- Foemiculum vulgare,
- isolation
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