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Citation: CHEN Li-Juan, ZHANG Sheng-Mao, WU Zhi-Shen, ZHANG Zhi-Jun, DANG Hong-Xin. Preparation and Characterization of ZnO Nanorods in Ionic Liquid[J]. Chinese Journal of Applied Chemistry, ;2005, 22(5): 554-556. shu

Preparation and Characterization of ZnO Nanorods in Ionic Liquid

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a Key Laboratory of Special Functional Materials, Henan University, Kaifeng 475001;
2.
b State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000

Corresponding author: WU Zhi-Shen,
Received Date: 2 August 2004
Available Online: 28 December 2004
Fund Project: 国家自然科学基金(20401006) (20401006)河南大学科学研究基金(XK02l04)资助项目 (XK02l04)

ZnO nanorods were successfully synthesized by thermal decomposition of Zn(OH)₂ in the ionic liquid 1-buty -3-ethylimidazolium tetrafluoroborate,and the growth mechanism of ZnO micro-crystallites was presumed.Their structure and morphology were characterized by means of transmission electron microscopy (TEM),infrared spectroscopy (IR),and X-ray powder diffraction (XRD).The TEM results indicate that the diameters and lengths of the ZnO nanorods were ca.25 nm and ca.150 nm,respectively.The IR spectra show that the ZnO nanorods were modified by 1-butyl-3-ethylimidazolium tetrafluoroborate.The XRD pattern reveals that the prepared ZnO nanorods belong to the hexagonal crystal system.The above-mentioned results indicate that ionic liquid can not only act as a reaction medium but also modify ZnO nanorods in the reaction.
- ionic liquids ZnO nanorod,
- thermal decomposition,
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