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Citation: GUO Zhi-An, ZHANG Xiao-Hui, ZHAO Jing-Chan, LIANG Xiao-Yun. Quantitative Analysis of Organic Acids in Electroless Plating Solution by Ion Suppression Chromatography[J]. Chinese Journal of Applied Chemistry, ;2006, 23(4): 386-389. shu

Quantitative Analysis of Organic Acids in Electroless Plating Solution by Ion Suppression Chromatography

1.
Department of Chemistry, Northwest University, Xi'an 710069

Corresponding author: GUO Zhi-An,
Received Date: 2 June 2005
Available Online: 9 November 2005
Fund Project: 陕西省自然科学基金(2003B013) (2003B013)陕西省教委基金(03JK075)资助项目 (03JK075)

A method for the analysis of 4 organic acids(aminoacetic acid,lactic acid,acetic acid, citric acid) in electroless plating solutions was developed.The analysis could be finished within 6 min.It is based on an ion suppression chromatographic separation under the conditions of isocratic elution with 25 m mol/L phosphate buffer solution(pH=2.1) on a Hypersil ODS column,and UV detection at 210 nm.Linear calibrations were obtained within 0.05×10^-3~5×10^-3 g/mL(r>0.999 4).The limits of detection(mg/L) were 6 of aminoacetic acid,20 for lactic acid,14 for acetic acid and 9 for citric acid,respectively.The average recovery rate was(n=6) 98.12%~102.60%,and the relative standard deviation(n=6) 0.31%~0.98%.Through the formula for distribution coefficient,and with the pH value of the original solution,the contents of different forms of each organic acid were figured out.
- ion suppression chromatography,
- electroless plating solution,
- organic acid,
- form analysis
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