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Citation: GAO Yong, TIAN Min, ZHANG Bin, ZHANG Min, GUO Zhao-qi, SHI Zhen. A New Synthesis Route for Precursor of 8-Amino-3,6-Dioxaoctanoic Acid[J]. Chinese Journal of Applied Chemistry, ;2006, 23(8): 918-920. shu

A New Synthesis Route for Precursor of 8-Amino-3,6-Dioxaoctanoic Acid

1.
Department of Chemistry, Northwest University, Xi'an 710069

Corresponding author: SHI Zhen,
Received Date: 16 September 2005
Available Online: 28 October 2005
Fund Project: 国家自然科学基金资助项目(20472067) (20472067)

A novel route was employed to synthesize 8-phthalimido-3,6-dioxaoctan-1-ol(3) from triethylene glycol.The experimental results show that route Ⅱ is an economical one.The total yield of 8-amino-3,6-dioxaoctanoic acid(5) by route Ⅱ is 36%.
- triethylene glycol,
- p-toluenesulfonyl triethylene glycol,
- phthalimido-dioxaoctan-ol,
- amino-dioxaoctanoic acid,
- synthesis
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