Citation: You Ming ZHANG, Ai Ru LU, Lian Xiang ZHAN, G, Wan Tian ZHAO, Liu Fang WANG. STUDIES ON COMPLEXES OF RARE EARTHS WITH CROWN ETHERS(V)-SYNTHESIS AND CHARACTERIZATION OF THE COMPLEXES OF RARE EARTH NITRATES WITH 2,2'-DINITRO-4,5,4',5'-BIS-(15-CROWN-5)-DIBENZO DISULFIDE[J]. Chinese Chemical Letters, ;1992, 3(6): 423-424. shu

STUDIES ON COMPLEXES OF RARE EARTHS WITH CROWN ETHERS(V)-SYNTHESIS AND CHARACTERIZATION OF THE COMPLEXES OF RARE EARTH NITRATES WITH 2,2'-DINITRO-4,5,4',5'-BIS-(15-CROWN-5)-DIBENZO DISULFIDE

a Department of Chemistry Northwest Normal University 730070;
b Department of Chemistry Lanzhou University 730000

Received Date: 27 January 1992

Three new solid complexes of macrocyclic polyether ligand 2, 2'-dinitro-4, 5, 4', 5'bis-(15-crown-5)-dihenzo disulfide(L) with trivalent rare earth nitrates having composition of RE(NO₃)₃ړLړ6H₂O(RE=Ce, Pr, Nd) have been synthesized in acetonitrile.All the isolated complexes have beencharacterized by elementary analysis, IR and UV spectra, differential thermal and thermogravimetricanalysis, X-ray powder diffraction analysis, molar conductance and measurements of solubility insome general solvents
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