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Citation: XU Zhen, LI Juan, LI Xinjun. Effect of NixCo3-xO4 Modification for CdSe/TiO2 Nanotube Arrays on Activity of Photoelectrochemical Oxidation of Water[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(3): 429-436. doi: 10.3969/j.issn.1001-4861.2013.00.051 shu

Effect of NixCo3-xO4 Modification for CdSe/TiO2 Nanotube Arrays on Activity of Photoelectrochemical Oxidation of Water

  • 1.

    1. Key Laboratory of Renewable Energy and Gas Hydrate, Guangzhou Institute of Energy Conversion, Chinese Academy of Sciences, Guangzhou 510640, China;

  • Received Date: 21 June 2012
    Available Online: 10 August 2012

    Fund Project: 国家自然科学基金(No.51172233) (No.51172233)国家重点基础研究发展计划项目(973)(2009CB220002)资助项目。 (973)(2009CB220002)

  • CdSe/TiO2 nanotube array (TiO2NTA) film was modified by NixCo3-xO4 through the method of ammonia-evaporation induction growth. The films were characterized by X-ray diffraction, field emission scanning electron microscopy, energy dispersive spectroscopy, X-ray photoelectron spectroscopy and UV-Vis diffuse reflectance spectroscopy. To characterize the photoanodes activity of photoelectrochemical oxidation of water, the chopped linear sweep voltammetry was performed in a three-electrode system under simulated solar irradiation. The results show that CdSe/TiO2NTA is covered by a thin layer of NixCo3-xO4 with the spinel structure in which Ni and Co are both in divalent and trivalent states. The modification of NixCo3-xO4 on the CdSe/TiO2NTA can lower the overpotential of water oxidation by about 430 mV compared with the CdSe/TiO2NTA. The introduction of Ni into the structure of Co3O4 leads to the surface enhancement of trivalent cations (Ni3+ and Co3+) and consequently facilitates the oxidation of water.
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