Citation:
ZHANG Jiang, ZHAO Yan-ming. Synthesis, Structure and Growth Mechanism of Magnesium Borate Nanobelts[J]. Acta Physico-Chimica Sinica,
;2006, 22(01): 110-113.
doi:
10.3866/PKU.WHXB20060122
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Magnesium borate nanobelts, a new kind of quasi one-dimensional nanomaterials, has been synthesized by heating mixed powders of crystalline boron and M nanoparticles in the presence of H2O at 1100 ℃. The produced white sample was characterized by different techniques, such as the X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive spectroscopy (EDS) and Fourier transform infrared spectroscopy (FT-IR). The results show that the products are single-crystalline Mg3B2O6Mg3B2O6 nanobelts except some attached Mg2B2O5 particles. The widths of the nanobelts are in the range of 100~200 nm and the lengths are up to several ten micrometers. The growth direction of the nanobelts nears to crystalline Mg3B2O6[010] direction. Finally, the growth mechanism for these novel Mg3B2O6 nanobelts and the effect of reactive temperature on the products have been primarily presented.
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