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Citation: Li Bo, Bao Chao, Shi Bai-Xuan, Tomonori Kawakami, Mitsuo Hiramatsu. Preparation and Formation Mechanism of Polycrystalline Vanadyl Phthalocyanine Nanoparticles[J]. Acta Physico-Chimica Sinica, ;2002, 18(12): 1057-1061. doi: 10.3866/PKU.WHXB20021201 shu

Preparation and Formation Mechanism of Polycrystalline Vanadyl Phthalocyanine Nanoparticles

1.
State Key Laboratory of Modern Optical Instrumentation, Zhejiang University, Hangzhou　310027;Central Research Laboratory, Hamamatsu Photonics K.K., 5000, Hirakuchi,Hamakita, Shizuoka　434-8601, Japan

Received Date: 18 February 2002
Available Online: 15 December 2002

The polycrystalline vanadyl phthalocyanine (VOPc) nanoparticles in phase I and phase II have been fabricated by laser ablation in aqueous solution without or with a kind of nonionic surfactants respectively. X-ray diffraction patterns, UV-Vis absorption spectroscopy and Fourier-transform infrared (FT-IR) spectroscopy have been used to characterize the crystalline structures in VOPc nanoparticles. About 100 nm-sized in phase I and 60 nm-sized in phase II particles of VOPc are observed by a scanning electron microscope (SEM). The formation mechanism of VOPc nanoparticles in phase II is discussed in this paper.
- Nanoparticles;Laser ablation;Surfactant;Phthalocyanine
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