Citation:
Wei Shi-Qiang, Zhang Xin-Yi, Liu Wen-Han, Wang Xiao-Guang, Yang Hong-Wei, Yan Wen-Sheng. Structural Study of Ni-B Ultrafine Amorphous Alloy during Annealed Crystallization[J]. Acta Physico-Chimica Sinica,
;2001, 17(08): 750-752.
doi:
10.3866/PKU.WHXB20010817
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Xray absorption fine structure (XAFS) and Xray diffraction (XRD) have been combined to investigate the structure of NiB ultrafine amorphous alloy prepared by chemical reduction during the crystallization process. The results demonstrate that a fcclike nanocrystalline Ni phase with a mediumrange order and a nanocrystalline Ni3B alloy are formed at 573 K where the first exothermic process is observed. At annealing temperature of 773 K, large amount of NiB ultrafine amorphous alloy decomposes into metal Ni.
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Keywords:
- XAFS;XRD;Ni-B ultraine amorphous alloy
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