Citation: Xiaomei Ning, Liang Zhan, Xiaosong Zhou, Jin Luo, Xunfu Zhou, Cuifen Luo. Preparation and Electro-Oxidation Performance of PtBi Supported on Carbon Cloth: A Recommended Comprehensive Chemical Experiment[J]. University Chemistry, ;2024, 39(11): 217-224. doi: 10.3866/PKU.DXHX202401085 shu

Preparation and Electro-Oxidation Performance of PtBi Supported on Carbon Cloth: A Recommended Comprehensive Chemical Experiment

Key Laboratory of Clean Energy Materials Chemistry of Guangdong Higher Education Institutes, School of Chemistry and Chemical Engineering, Lingnan Normal University, Zhanjiang 524048, Guangdong Province, China

Received Date: 30 January 2024
Revised Date: 3 April 2024

In this experiment, we prepared, characterized, and utilized PtBi supported on carbon cloth as a self-supporting electrode for electro-oxidation applications. The aim was to promote the integration of science and education and foster the development of innovative talents. Through this experiment, students can gain a better understanding of electrochemical devices and energy conversion in Physical Chemistry, as well as catalyst performance evaluation criteria. It also aims to stimulate students’ interest in scientific research and equip them with essential laboratory skills such as the preparation, characterization, and electrochemical testing of nanomaterials. This experiment aims to enhance students’ scientific literacy and improve their ability to analyze performance data, comprehend electro-oxidation reaction processes, and understand electrode processes using electrochemical and kinetic concepts.
- Carbon cloth,
- PtBi catalyst,
- Electro-oxidation,
- Comprehensive chemical experiment
1. [1]
2. [2]
3. [3]
  Zhang, Q.; Suresh, L.; Liang, Q.; Zhang, Y.; Yang, L.; Paul, N.; Tan, S. C. Adv. Sustainable Syst. 2021, 5 (3), 2000152.
4. [4]
  Ning, X.; Zhou, X.; Luo, J.; Ma, L.; Xu, X.; Zhan, L. Electrochim. Acta 2019, 319, 129.
5. [5]
6. [6]
  Zhou, Y.; Shen, Y.; Xi, J. Appl. Catal. B:Environ. 2019, 245, 604.
7. [7]
  Wang, Y.; He, Y.; Zhou, M. Appl. Surf. Sci. 2019, 479, 1270.
8. [8]
  Ghiabi, C.; Ghaffarinejad, A.; Kazemi, H.; Salahandish, R. Renew. Energy 2018, 126, 1085.
9. [9]
  Costa Santos, J. B.; Vieira, C.; Crisafulli, R.; Linares, J. J. Int. J. Hydrog. Energy 2020, 45 (47), 25658.
10. [10]
  Wang, Z.; Zhou, S.; Liao, W.; Wang, Q. Int. J. Hydrog. Energy 2022, 47 (36), 16056.
11. [11]
  Zhan, C.; Bu, L.; Sun, H.; Huang, X.; Zhu, Z.; Yang, T.; Ma, H.; Li, L.; Wang, Y.; Geng, H.; et al. Angew. Chem. Int. Ed. 2023, 62 (3), e202213783.
12. [12]
13. [13]
  Ning, X.; Zhan, L.; Zhou, X.; Luo, J.; Wang, Y. J. Colloid Interface Sci. 2024, 655, 920.
1. [1]
  Huirong BAO , Jun YANG , Xiaomiao FENG . Preparation and electrochemical properties of NiCoP/polypyrrole/carbon cloth by electrodeposition. Chinese Journal of Inorganic Chemistry, 2025, 41(6): 1083-1093. doi: 10.11862/CJIC.20250008
2. [2]
  Bin Liu . Teaching case design of chemistry “101 Plan” syntheticchemistry experiment course: taking the experiment of preparation of platinum nanocatalyst supported on carbon and determination of its electrochemical catalytic performance of methanol oxidation as an example. University Chemistry, 2026, 41(6): 125-135. doi: 10.12461/PKU.DXHX202506043
3. [3]
  Hua Zhou , Yuqing Li , Rui Zhang , Jialong Qian , Zhenhua Li , Mingfei Shao . 电解水制氢耦合5-羟甲基糠醛氧化制2,5-呋喃二甲酸创新实验设计. University Chemistry, 2026, 41(8): 321-330. doi: 10.12461/PKU.DXHX202507123
4. [4]
  Jinyi Sun , Lin Ma , Yanjie Xi , Jing Wang . Preparation and Electrocatalytic Nitrogen Reduction Performance Study of Vanadium Nitride@Nitrogen-Doped Carbon Composite Nanomaterials: A Recommended Comprehensive Chemistry Experiment. University Chemistry, 2024, 39(4): 184-191. doi: 10.3866/PKU.DXHX202310094
5. [5]
  Fangfang Tan , Lele Zhang , Penghua Jing , Pengju Zhao , Yang Li . 烯烃光催化氧化制备二苯甲酮——介绍一个绿色合成综合实验. University Chemistry, 2026, 41(8): 380-388. doi: 10.12461/PKU.DXHX202507049
6. [6]
  Yanan Liu , Yufei He , Dianqing Li . Preparation of Highly Dispersed LDHs-based Catalysts and Testing of Nitro Compound Reduction Performance: A Comprehensive Chemical Experiment for Research Transformation. University Chemistry, 2024, 39(8): 306-313. doi: 10.3866/PKU.DXHX202401081
7. [7]
  Yihan Xue , Jie Zhang , Xiaoru Wen . Electrodeposited FeOOH self-supported electrode for CDI rare-earth wastewater treatment: a comprehensive physical chemistry experiment. University Chemistry, 2026, 41(6): 404-414. doi: 10.12461/PKU.DXHX202509023
8. [8]
  Xin Zhou , Zhi Zhang , Yun Yang , Shuijin Yang . A Study on the Enhancement of Photocatalytic Performance in C/Bi/Bi₂MoO₆ Composites by Ferroelectric Polarization: A Recommended Comprehensive Chemical Experiment. University Chemistry, 2024, 39(4): 296-304. doi: 10.3866/PKU.DXHX202310008
9. [9]
  Haihua Yang , Minjie Zhou , Binhong He , Wenyuan Xu , Bing Chen , Enxiang Liang . Synthesis and Electrocatalytic Performance of Iron Phosphide@Carbon Nanotubes as Cathode Material for Zinc-Air Battery: a Comprehensive Undergraduate Chemical Experiment. University Chemistry, 2024, 39(10): 426-432. doi: 10.12461/PKU.DXHX202405100
10. [10]
  Chao Zeng , Pengwei Zeng . Photocatalytic-Fenton degradation of Rhodamine B using sulfidized FeOCl: a proposed comprehensive chemical experiment. University Chemistry, 2026, 41(7): 300-308. doi: 10.12461/PKU.DXHX202506057
11. [11]
  Sen Lin , Rong Jiang , Xuefeng Lu , Guohui Jiang , Kaining Ding , Jinshui Zhang , Xinchen Wang . Promoting the Integration of Science and Education through Digital Intelligence Technology: Data-Driven Development of Efficient Water Electrolysis Catalysts in Comprehensive Chemical Experiment Teaching. University Chemistry, 2026, 41(1): 188-203. doi: 10.12461/PKU.DXHX202505090
12. [12]
  Xianggui Kong , Wenying Shi . Comprehensive Chemical Experimental Design of Optically Encrypted Materials. University Chemistry, 2025, 40(3): 355-362. doi: 10.12461/PKU.DXHX202406067
13. [13]
  Jianfeng Yan , Yating Xiao , Xin Zuo , Caixia Lin , Yaofeng Yuan . Comprehensive Chemistry Experimental Design of Ferrocenylphenyl Derivatives. University Chemistry, 2024, 39(4): 329-337. doi: 10.3866/PKU.DXHX202310005
14. [14]
  Haoxiang Zhang , Zhihan Zhao , Yongchen Jin , Zhiqiang Niu , Jinlei Tian . Synthesis of an Efficient Absorbent Gel: A Recommended Comprehensive Chemistry Experiment. University Chemistry, 2024, 39(11): 251-258. doi: 10.12461/PKU.DXHX202401084
15. [15]
  Yunqiang Sun , Xiaowei Hu , Tingting He , Hongjiao Nie , Qiying Xia . 基于创新能力培养的综合化学实验教学改革与实践. University Chemistry, 2026, 41(10): 90-97. doi: 10.12461/PKU.DXHX202510091
16. [16]
  Li Li , Lin Li , Qifei Wang , Yang Wang , Yupeng Guo . 纳米纤维膜制备及油水分离应用——科教融合综合化学实验. University Chemistry, 2026, 41(10): 344-353. doi: 10.12461/PKU.DXHX202510062
17. [17]
  Jinfeng Chu , Yicheng Wang , Ji Qi , Yulin Liu , Yan Li , Lan Jin , Lei He , Yufei Song . Comprehensive Chemical Experiment Design: Convenient Preparation and Characterization of an Oxygen-Bridged Trinuclear Iron(III) Complex. University Chemistry, 2024, 39(7): 299-306. doi: 10.3866/PKU.DXHX202310105
18. [18]
  Guang Huang , Lei Li , Dingyi Zhang , Xingze Wang , Yugai Huang , Wenhui Liang , Zhifen Guo , Wenmei Jiao . Cobalt’s Valor, Nickel’s Foe: A Comprehensive Chemical Experiment Utilizing a Cobalt-based Imidazolate Framework for Nickel Ion Removal. University Chemistry, 2024, 39(8): 174-183. doi: 10.3866/PKU.DXHX202311051
19. [19]
  Wenxu Liu , Feng Han , Boxuan Wang , Huayi Liu , Xiaobin Gu , Xin Zhang , Yao Liu . Comprehensive Chemical Experiment: Design, Synthesis, and Photoelectronic Properties Study of Fully Non-Fused Ring Electron Acceptors. University Chemistry, 2025, 40(10): 263-275. doi: 10.12461/PKU.DXHX202412021
20. [20]
  Jiayi Wu , Yaping Wang , Jijun Jiang , Mei Pan , Chengyong Su . Case design of the Chemistry “101 Plan” comprehensive chemistry experiment: taking laser confocal cell imaging of MOC-16 as an example. University Chemistry, 2026, 41(6): 166-174. doi: 10.12461/PKU.DXHX202605044

Get Citation

PDF

XML

Metrics

PDF Downloads(1)
Abstract views(2074)
HTML views(285)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142