Citation: Tian He,  Jingtao Ye,  Yang Li,  Shouchun Yin. Lead by “Practice and Use” with a Loud Voice: A Comprehensive Experiment of the Synthesis and Photothermal Performance of Water-Soluble Near-Infrared Organic Nanomaterials[J]. University Chemistry, ;2023, 38(5): 143-148. doi: 10.3866/PKU.DXHX202207155 shu

Lead by “Practice and Use” with a Loud Voice: A Comprehensive Experiment of the Synthesis and Photothermal Performance of Water-Soluble Near-Infrared Organic Nanomaterials

  • Near-infrared (NIR) plays a vital role in the fields of photothermal therapy, bioimaging, photodynamic therapy, and medical diagnosis. In this comprehensive experiment, organic nanoparticles based on electron-transfer complexes (viz., coronene (COR) and 7,7,8,8-tetracyano-p-benzoquinonedimethane (TCNQ)) were prepared via precipitation. Absorption in the NIR regions was determined using ultraviolet-visible spectrophotometry, and the structure of the nanoparticles was analyzed using dynamic light scattering and transmission electron microscopy. The photothermal properties of the nanoparticles were evaluated via infrared thermal imaging. This study applies the frontier of scientific research to experimental teaching, which helps students to consolidate their scientific knowledge, improve their experimental skills and laboratory safety consciousness, broaden their scientific research vision, and instill the exploration spirit of scientific theoretical research with the ultimate goal of application “landing”.
  • 加载中
    1. [1]

    2. [2]

    3. [3]

    4. [4]

    5. [5]

      Li, S.; Deng, Q.; Zhang, Y.; Li, X.; Wen, G.; Cui, X.; Wan, Y.; Huang, Y.; Chen, J.; Liu, Z.; et al. Adv. Mater. 2020, 32, 2001146.

    6. [6]

      Liu, S.; Li, Y.; Kwok, R. T. K.; Lam, J. W. Y.; Tang B. Z. Chem. Sci. 2021, 12, 3427.

    7. [7]

      Liang, Y.; Zhang, H.; Yuan, H.; Lu, W.; Li, Z.; Wang L.; Gao, L. H. ACS Appl. Bio Mater. 2020, 3, 3494.

    8. [8]

      Li, X.; Fang, F.; Sun, B.; Yin, C.; Tan, J.; Wan, Y.; Zhang, J.; Sun, P.; Fan, Q.; Wang, P.; et al. Nanoscale Horiz. 2021, 6, 177.

    9. [9]

      Jiang, Y.; Li, J.; Zhen, X.; Xie, C.; Pu, K. Adv. Mater. 2018, 30, 1705980.

    10. [10]

      Li, X.; Liu, L.; Li, S.; Wan, Y.; Chen, J. X.; Tian, S.; Huang, Z.; Xiao, Y. F.; Cui, X.; Xiang, C.; et al. ACS Nano 2019, 13, 12901.

    11. [11]

      Tian, S.; Bai, H. T.; Li, S. L.; Xiao, Y. F.; Cui, X.; Li, X. Z.; Tan, J. H.; Huang, Z. M.; Shen, D.; Liu, W. M.; et al. Angew. Chem. Int. Ed. 2021, 60, 11758.

    12. [12]

      Lyu, Y.; Xie, C.; Chechetka, S. A.; Miyako, E.; Pu, K. J. Am. Chem. Soc. 2016, 138, 9049.

    13. [13]

      He, S.; Jiang, Y.; Li, J.; Pu, K. Angew. Chem. Int. Ed. 2020, 59, 10633.

    14. [14]

      Yang, K.; Xu, H.; Cheng, L.; Sun, C.; Wang, J.; Liu, Z. Adv. Mater. 2012, 24, 5586.

    15. [15]

      Sheng, Z.; Hu, D.; Zheng, M.; Zhao, P.; Liu, H.; Gao, D.; Gong, P.; Gao, G.; Zhang, P.; Ma, Y.; et al. ACS Nano 2014, 8, 12310.

    16. [16]

    17. [17]

  • 加载中
    1. [1]

      Ruonan LiShijie LiangYunhua XuCuifen ZhangZheng TangBaiqiao LiuWeiwei Li . Chlorine-Substituted Double-Cable Conjugated Polymers with Near-Infrared Absorption for Low Energy Loss Single-Component Organic Solar Cells. Acta Physico-Chimica Sinica, 2024, 40(8): 2307037-0. doi: 10.3866/PKU.WHXB202307037

    2. [2]

      Qi Wang Yicong Gao Feng Lu Quli Fan . Preparation and Performance Characterization of the Second Near-Infrared Phototheranostic Probe: A New Design and Teaching Practice of Polymer Chemistry Comprehensive Experiment. University Chemistry, 2024, 39(11): 342-349. doi: 10.12461/PKU.DXHX202404141

    3. [3]

      Juan Yuan Bin Zhang Jinping Wu Mengfan Wang . Design of a Comprehensive Experiment on Preparation and Characterization of Cu2(Salen)2 Nanomaterials with Two Distinct Morphologies. University Chemistry, 2024, 39(10): 420-425. doi: 10.3866/PKU.DXHX202402014

    4. [4]

      Xian BISisi WANGJinyue ZHANGYujia PENGZhen SHENHua LU . Discovery, development, and perspectives of circularly polarized luminescent materials based on β-isoindigo skeletons. Chinese Journal of Inorganic Chemistry, 2025, 41(6): 1049-1057. doi: 10.11862/CJIC.20240456

    5. [5]

      Xia Gao Huibin Pan Chengfang Qiao Fengying Chen Jun Wang Qian Liu . Teaching Reform and Practice of Chemistry Comprehensive Experiment Course under Professional Certification Background. University Chemistry, 2024, 39(10): 195-202. doi: 10.12461/PKU.DXHX202401078

    6. [6]

      Jiajia Wang Sibo Huang Xijing Gao Chaoxun Liu Haibo Zhang . 光催化硝酸根还原产氨的综合实验设计. University Chemistry, 2025, 40(8): 241-248. doi: 10.12461/PKU.DXHX202410050

    7. [7]

      Kun Xu Xinxin Song Zhilei Yin Jian Yang Qisheng Song . Comprehensive Experimental Design of Preferential Orientation of Zinc Metal by Heat Treatment for Enhanced Electrochemical Performance. University Chemistry, 2024, 39(4): 192-197. doi: 10.3866/PKU.DXHX202309050

    8. [8]

      Xiaofeng Xia Jielian Zhu . Innovative Comprehensive Experimental Design: Synthesis of 6-Fluoro-N-benzoyl Tetrahydroquinoline. University Chemistry, 2024, 39(10): 344-352. doi: 10.12461/PKU.DXHX202405063

    9. [9]

      Zunxiang Zeng Yuling Hu Yufei Hu Hua Xiao . Analysis of Plant Essential Oils by Supercritical CO2Extraction with Gas Chromatography-Mass Spectrometry: An Instrumental Analysis Comprehensive Experiment Teaching Reform. University Chemistry, 2024, 39(3): 274-282. doi: 10.3866/PKU.DXHX202309069

    10. [10]

      Jinrong Bao Jinglin Zhang Wenxian Li Xiaowei Zhu . 苯甲酸稀土配合物的制备及性能表征——基于应用化学专业人才培养的综合化学实验案例分析. University Chemistry, 2025, 40(8): 218-224. doi: 10.12461/PKU.DXHX202409142

    11. [11]

      Tianlong Zhang Rongling Zhang Hongsheng Tang Yan Li Hua Li . Online Monitoring and Mechanistic Analysis of 3,5-diamino-1,2,4-triazole (DAT) Synthesis via Raman Spectroscopy: A Recommendation for a Comprehensive Instrumental Analysis Experiment. University Chemistry, 2024, 39(6): 303-311. doi: 10.3866/PKU.DXHX202312006

    12. [12]

      Rong Tian Yadi Yang Naihao Lu . Comprehensive Experimental Design of Undergraduate Students Based on Interdisciplinarity: Study on the Effect of Quercetin on Chlorination Activity of Myeloperoxidase. University Chemistry, 2024, 39(8): 247-254. doi: 10.3866/PKU.DXHX202312064

    13. [13]

      Zufeng Qiu Jie Ouyang Yiru Wang Hengting Yang Xin Liao Chi Zhang Xuanyao Jiang Shunliu Deng Zhiwei Lin . 综合运用分析仪器解析“盲盒”样品——未知物的剖析. University Chemistry, 2025, 40(6): 296-302. doi: 10.12461/PKU.DXHX202405167

    14. [14]

      Yang Chen Peng Chen Yuyang Song Yuxue Jin Song Wu . Application of Chemical Transformation Driven Impurity Separation in Experiments Teaching: A Novel Method for Purification of α-Fluorinated Mandelic Acid. University Chemistry, 2024, 39(6): 253-263. doi: 10.3866/PKU.DXHX202310077

    15. [15]

      Yanyang Li Zongpei Zhang Kai Li Shuangquan Zang . Ideological and Political Design for the Comprehensive Experiment of the Synthesis and Aggregation-Induced Emission (AIE) Performance Study of Salicylaldehyde Schiff-Base. University Chemistry, 2024, 39(2): 105-109. doi: 10.3866/PKU.DXHX202307020

    16. [16]

      Feng Lu Tao Wang Qi Wang . Preparation and Characterization of Water-Soluble Silver Nanoclusters: A New Design and Teaching Practice in Materials Chemistry Experiment. University Chemistry, 2025, 40(4): 375-381. doi: 10.12461/PKU.DXHX202406005

    17. [17]

      Jiahui CHENTingting ZHENGXiuyun ZHANGWei LÜ . Research progress of near-infrared absorption inorganic nanomaterials in photothermal and photodynamic therapy of tumors. Chinese Journal of Inorganic Chemistry, 2024, 40(12): 2396-2414. doi: 10.11862/CJIC.20240106

    18. [18]

      Xue WuYupeng LiuBingzhe WangLingyun LiZhenjian LiQingcheng WangQuansheng ChengGuichuan XingSongnan Qu . Rationally assembling different surface functionalized carbon dots for enhanced near-infrared tumor photothermal therapy. Acta Physico-Chimica Sinica, 2025, 41(9): 100109-0. doi: 10.1016/j.actphy.2025.100109

    19. [19]

      Wei Li Jinfan Xu Yongjun Zhang Ying Guan . 共价有机框架整体材料的制备及食品安全非靶向筛查应用——推荐一个仪器分析综合化学实验. University Chemistry, 2025, 40(6): 276-285. doi: 10.12461/PKU.DXHX202406013

    20. [20]

      Feng Sha Xinyan Wu Ping Hu Wenqing Zhang Xiaoyang Luan Yunfei Ma . Design of Course Ideology and Politics for the Comprehensive Organic Synthesis Experiment of Benzocaine. University Chemistry, 2024, 39(2): 110-115. doi: 10.3866/PKU.DXHX202307082

Metrics
  • PDF Downloads(5)
  • Abstract views(834)
  • HTML views(107)

通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索
Address:Zhongguancun North First Street 2,100190 Beijing, PR China Tel: +86-010-82449177-888
Powered By info@rhhz.net

/

DownLoad:  Full-Size Img  PowerPoint
Return