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Citation: Yuting Tong, Jinyu Dai, Jianying Zhao, Runwei Wang. 综合性化学实验设计:中空介孔有机硅纳米材料制备与表征[J]. University Chemistry, ;2021, 36(4): 200411. doi: 10.3866/PKU.DXHX202004114 shu

综合性化学实验设计:中空介孔有机硅纳米材料制备与表征

1.
School of Chemical Engineering, Sichuan University, Chengdu 610065, China;
2.
State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of Chemistry, Jilin University, Changchun 130012, China;
3.
College of Chemistry and Chemical Engineering, Shandong University of Technology, Zibo 255049, Shandong Province, China

Received Date: 27 April 2020

本实验围绕中空介孔有机硅纳米材料前沿制备方法，采用逐层包覆与同步生长诱导腐蚀法相结合的方法，设计了一个简单、有效和可控的PMO系列材料制备的综合性教学实验，分别制备了单分散SiO₂纳米球和中空介孔有机硅纳米球（Et-HPMO），并通过红外光谱（IR）、扫描电镜（SEM）、透射电镜（TEM）及粉末X射线衍射（PXRD）表征纳米材料的化学组成、微观形貌及介孔结构。使学生学习PMO系列纳米材料的设计、制备及表征方法，提高学生的综合性和系统性实验技能，为学生从事先进材料制备打下基础。
- Periodic mesoporous organosilica,
- Nanomaterials,
- Integrated experiment
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