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Citation: BAI Yin-Juan, NAN Zhi-Xiang, LI Jun. Synthesis and Characterization of Acetylferrocene: Detailed Analysis of a Comprehensive Chemistry Experiment[J]. University Chemistry, ;2016, 31(8): 81-85. doi: 10.3866/PKU.DXHX201510011 shu

Synthesis and Characterization of Acetylferrocene: Detailed Analysis of a Comprehensive Chemistry Experiment

College of Chemistry & Materials Science, Northwest University, Xi'an 710127, P. R. China

The acetylation, purification and characterization of a typical comprehensive chemistry experiment "the synthesis and characterization of acetylferrocene" were described in this paper. The details of reactants addition, reaction temperature control, neutralization, TLC monitoring, column chromatography and characterization of the product with infrared spectrum and hydrogen nuclear magnetic resonance spectrum were investigated. Instruction for students on how to plan comprehensive chemistry experiment, improve the ability for observing, analyzing and solving problems were discussed.
- Acetylferrocene,
- Synthesis,
- Characterization,
- Comprehensive experiment
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