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磁性金属有机骨架-聚多巴胺的制备并用于水产养殖水样中阳离子染料的萃取检测

杨晓涵 ,  吴雯倩 ,  王彬 ,  林风 ,  吴小海 ,  卢昕

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引用本文: 杨晓涵, 吴雯倩, 王彬, 林风, 吴小海, 卢昕. 磁性金属有机骨架-聚多巴胺的制备并用于水产养殖水样中阳离子染料的萃取检测[J]. 色谱, 2020, 38(2): 195-205. doi: 10.3724/SP.J.1123.2019.05045 shu
Citation:  YANG Xiaohan,  WU Wenqian,  WANG Bin,  LIN Feng,  WU Xiaohai,  LU Xin. Preparation of magnetic metal-organic frameworks-polydopamine for extraction and detection of cationic dyes from water samples in a fishery[J]. Chinese Journal of Chromatography, 2020, 38(2): 195-205. doi: 10.3724/SP.J.1123.2019.05045 shu

磁性金属有机骨架-聚多巴胺的制备并用于水产养殖水样中阳离子染料的萃取检测

  • 药用资源化学与药物分子工程教育部重点实验室, 广西师范大学化学与药学学院, 广西 桂林 541004

    • 通讯作者: 卢昕, E-mail:luxin-chem@163.com
  • 基金项目:

    国家自然科学基金（21565008）.

摘要: 利用多巴胺（DA）中的儿茶酚基团能与金属有机骨架晶体（MOFs）中金属离子螯合的原理，以ZIF-67为模板，经DA蚀刻-自聚合形成具有孔洞结构的聚多巴胺（PDA）壳层，制备了磁性-MOFs-PDA（Fe3O4@Z67D）新型材料。多种表征手段验证了材料的形貌、结构和性能。新型材料具有亲水性的表面、纳米级的孔径，以及良好的磁响应，被用作磁固相萃取吸附剂。结合高效液相色谱分析手段，建立了萃取检测亚甲蓝（MB）和结晶紫（CV）两种阳离子染料的新方法。在最优的萃取和色谱分析条件下，MB和CV的线性范围分别为0.5~200 μ g/L和0.01~50 μ g/L，检出限分别为0.04 μ g/L和0.008 μ g/L，对两种染料的富集因子分别为777和688。新型材料重复使用10次，其萃取性能未见发生变化。该方法成功应用于检测淡水鱼养殖用水中痕量的MB和CV，加标回收率为82.0%~109.0%，RSD低于2.9%。

English

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  • 收稿日期:  2019-05-30
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