磁性金属有机骨架-聚多巴胺的制备并用于水产养殖水样中阳离子染料的萃取检测

杨晓涵 吴雯倩 王彬 林风 吴小海 卢昕

引用本文: 杨晓涵,  吴雯倩,  王彬,  林风,  吴小海,  卢昕. 磁性金属有机骨架-聚多巴胺的制备并用于水产养殖水样中阳离子染料的萃取检测[J]. 色谱, 2020, 38(2): 195-205. doi: 10.3724/SP.J.1123.2019.05045 shu
Citation:  YANG Xiaohan,  WU Wenqian,  WANG Bin,  LIN Feng,  WU Xiaohai,  LU Xin. Preparation of magnetic metal-organic frameworks-polydopamine for extraction and detection of cationic dyes from water samples in a fishery[J]. Chinese Journal of Chromatography, 2020, 38(2): 195-205. doi: 10.3724/SP.J.1123.2019.05045 shu

磁性金属有机骨架-聚多巴胺的制备并用于水产养殖水样中阳离子染料的萃取检测

  • 基金项目:

    国家自然科学基金(21565008).

摘要: 利用多巴胺(DA)中的儿茶酚基团能与金属有机骨架晶体(MOFs)中金属离子螯合的原理,以ZIF-67为模板,经DA蚀刻-自聚合形成具有孔洞结构的聚多巴胺(PDA)壳层,制备了磁性-MOFs-PDA(Fe3O4@Z67D)新型材料。多种表征手段验证了材料的形貌、结构和性能。新型材料具有亲水性的表面、纳米级的孔径,以及良好的磁响应,被用作磁固相萃取吸附剂。结合高效液相色谱分析手段,建立了萃取检测亚甲蓝(MB)和结晶紫(CV)两种阳离子染料的新方法。在最优的萃取和色谱分析条件下,MB和CV的线性范围分别为0.5~200 μg/L和0.01~50 μg/L,检出限分别为0.04 μg/L和0.008 μg/L,对两种染料的富集因子分别为777和688。新型材料重复使用10次,其萃取性能未见发生变化。该方法成功应用于检测淡水鱼养殖用水中痕量的MB和CV,加标回收率为82.0%~109.0%,RSD低于2.9%。

English

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  • 收稿日期:  2019-05-30
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