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Citation: LI You, YU Hongwei, WANG Fei. Determination of perchlorate in wine by ion chromatography[J]. Chinese Journal of Chromatography, ;2016, 34(10): 989-991. doi: 10.3724/SP.J.1123.2016.05032 shu

Determination of perchlorate in wine by ion chromatography

LI You ^1, ,
YU Hongwei ¹ ,
WANG Fei ²

1.
Metrohm China Limited Company, Beijing 100101, China;
2.
Qinhuangdao Entry-Exit Inspection and Quarantine Bureau, Qinghuangdao 066004, China

Received Date: 30 May 2016

An ion chromatographic method was developed for the determination of perchlorate in wine. The content of perchlorate in four kinds of wine was determined. Metrosep A Supp5 column (150 mm×4.0 mm) was used for the separation with the eluent of 1.0 mmol/L Na₂CO₃-acetone (85 : 15, v/v) at the flow rate of 0.8 mL/min, and the column temperature was 40℃. Perchlorate had good linearity in the range of 0.1-10.0 mg/L. The recoveries of the method were more than 86.0%, and the relative standard deviations were less than 2.6%. The method is simple and rapid, and can be used for the determination of perchlorate in wine.
- ion chromatography (IC),
- perchlorate,
- wine
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