Citation: BAI Junying, HUANG Renhua, LU Yunmei, YU You, WANG Dan. Optimization of headspace solid phase micro-extraction combined with gas chromatography-mass spectrometry conditions of volatile flavor from Feijoa sellowiana leaves[J]. Chinese Journal of Chromatography, ;2016, 34(8): 778-782. doi: 10.3724/SP.J.1123.2016.04006 shu

Optimization of headspace solid phase micro-extraction combined with gas chromatography-mass spectrometry conditions of volatile flavor from Feijoa sellowiana leaves

1.
College of Life Science and Engineering, Southwest University of Science and Technology, Mianyang 621010, China

Corresponding author: HUANG Renhua,
Received Date: 5 April 2016

Fund Project:

To establish the appropriate extraction conditions for the analysis of volatile constituents from Feijoa sellowiana leaves by headspace solid phase micro-extraction (HS-SPME) combined with gas chromatography-mass spectrometry (GC-MS), the extraction conditions were investigated by orthogonal tests. The sum of the peak areas and total peak numbers of the volatile constituents were used as indices to optimize the extraction conditions by using L₉(3⁴) orthogonal array design. The results showed that the influence of temperature was larger and that of the sample amount was smaller for total peak numbers and peak areas. The optimum HS-SPME parameters were selected as follows: 0.6 g sample, extracted for 50 min at 50 ℃, and then desorbed for 6 min. Under these conditions, a total of 88 substances were detected. These substances can reflect the fragrant chemical components of Feijoa sellowiana leaves, and provide some references for the development and utilization of the leaves.
1. [1]
  [1] Jiang S X, Feng J J. Chinese Journal of Chromatography, 2012, 30(3): 219 蒋生祥, 冯娟娟. 色谱, 2012, 30(3): 219
2. [2]
  [2] Geppert H. Anal Chem, 1998, 70: 3981
3. [3]
  [3] Xiao D. Chinese Journal of Public Health Engineering, 2015, 14(1): 88 肖丹. 中国卫生工程学, 2015, 14(1): 88
4. [4]
  [4] Yan K L, Lin L Q, Zheng X X, et al. Chinese Journal of Chromatography, 2013, 31(7): 634 严矿林, 林丽琼, 郑夏汐, 等. 色谱, 2013, 31(7): 634
5. [5]
  [5] Liu Q, Shen M Y, Nie S P, et al. Food Science, 2015, 36(22): 102 刘倩, 申明月, 聂少平, 等. 食品科学, 2015, 36(22): 102
6. [6]
  [6] Chen Y, Dao X, Tan L, et al. Physical Testing and Chemical Analysis Part B: Chemical Analysis, 2015, 51(8): 1174 陈烨, 刀谞, 谭丽, 等. 理化检验:化学分册, 2015, 51(8): 1174
7. [7]
  [7] Cui Y H, Yao W X, Zhang S L, et al. Journal of Instrumental Analysis, 2015, 34(4): 375 崔艳华, 姚伟宣, 张素玲, 等. 分析测试学报, 2015, 34(4): 375
8. [8]
  [8] Ruberto G, Tringali C. Phytochemistry, 2004, 65(21): 2947
9. [9]
  [9] Nodari R O, Guerra M P, Meler K, et al. Acta Hort, 1997, 452: 41
10. [10]
  [10] El-Shenawy S M, Marzouk M S, El-Dib R A, et al. Rev Latino Quim, 2008, 36(3): 103
11. [11]
  [11] Saj O P, Roy R K, Savitha S V. J Pure Appl Microbio, 2008, 2(1): 227
12. [12]
  [12] Beyhan Ö, Elmastas M, Gedikli F. J Med Plants Res, 2010, 4(11): 1065
13. [13]
  [13] Wang D, Yuan X H, Xiong S L, et al. Journal of Food Science and Biotechnology, 2015(4): 337 王丹, 袁小红, 熊双丽, 等. 食品与生物技术学报, 2015(4): 337
14. [14]
  [14] Zhang X J, Zhao Z H, Zhang Z L, et al. Chinese Journal of Experimental Traditional Medical Formulae, 2014, 20(21): 66 张小俊, 赵志鸿, 张壮丽, 等. 中国实验方剂学杂志, 2014, 20(21): 66
15. [15]
  [15] Jia K, Hu X S, Liao X J, et al. Food Science, 2010, 31(10): 239 贾恺, 胡小松, 廖小军, 等. 食品科学, 2010, 31(10): 239
16. [16]
  [16] Xue Y J, Zhang L, Feng L, et al. Science and Technology of Food Industry, 2015(1): 328 薛妍君, 张丽, 冯莉, 等. 食品工业科技, 2015(1): 328
1. [1]
  Zunxiang Zeng , Yuling Hu , Yufei Hu , Hua Xiao . Analysis of Plant Essential Oils by Supercritical CO₂Extraction with Gas Chromatography-Mass Spectrometry: An Instrumental Analysis Comprehensive Experiment Teaching Reform. University Chemistry, 2024, 39(3): 274-282. doi: 10.3866/PKU.DXHX202309069
2. [2]
  Siwei Hou , Yaxin Niu , Guanglu Zhang , Yanmei Yang , Xu Wang , Zhenzhen Chen . Application of Solid-Phase Microextraction and Mass Spectrometry in Environmental Detection. University Chemistry, 2026, 41(3): 297-306. doi: 10.12461/PKU.DXHX202504078
3. [3]
  Yanhui Zhong , Ran Wang , Zian Lin . Analysis of Halogenated Quinone Compounds in Environmental Water by Dispersive Solid-Phase Extraction with Liquid Chromatography-Triple Quadrupole Mass Spectrometry. University Chemistry, 2024, 39(11): 296-303. doi: 10.12461/PKU.DXHX202402017
4. [4]
  Shunü Peng , Huamin Li , Zhaobin Chen , Yiru Wang . Simultaneous Application of Multiple Quantitative Analysis Methods in Gas Chromatography for the Determination of Active Ingredients in Traditional Chinese Medicine Preparations. University Chemistry, 2025, 40(10): 243-249. doi: 10.12461/PKU.DXHX202412043
5. [5]
  Ke Qiu , Fengmei Wang , Mochou Liao , Kerun Zhu , Jiawei Chen , Wei Zhang , Yongyao Xia , Xiaoli Dong , Fei Wang . A Fumed SiO₂-based Composite Hydrogel Polymer Electrolyte for Near-Neutral Zinc-Air Batteries. Acta Physico-Chimica Sinica, 2024, 40(3): 2304036-0. doi: 10.3866/PKU.WHXB202304036
6. [6]
  Xiaowu Zhang , Pai Liu , Qishen Huang , Shufeng Pang , Zhiming Gao , Yunhong Zhang . Acid-Base Dissociation Equilibrium in Multiphase System: Effect of Gas. University Chemistry, 2024, 39(4): 387-394. doi: 10.3866/PKU.DXHX202310021
7. [7]
  Chongjing Liu , Yujian Xia , Pengjun Zhang , Shiqiang Wei , Dengfeng Cao , Beibei Sheng , Yongheng Chu , Shuangming Chen , Li Song , Xiaosong Liu . Understanding Solid-Gas and Solid-Liquid Interfaces through Near Ambient Pressure X-Ray Photoelectron Spectroscopy. Acta Physico-Chimica Sinica, 2025, 41(2): 100013-0. doi: 10.3866/PKU.WHXB202309036
8. [8]
  Runjie Li , Hang Liu , Xisheng Wang , Wanqun Zhang , Wanqun Hu , Kaiping Yang , Qiang Zhou , Si Liu , Pingping Zhu , Wei Shao . 氨基酸的衍生及手性气相色谱分离创新实验. University Chemistry, 2025, 40(6): 286-295. doi: 10.12461/PKU.DXHX202407059
9. [9]
  Jiao CHEN , Yi LI , Yi XIE , Dandan DIAO , Qiang XIAO . Vapor-phase transport of MFI nanosheets for the fabrication of ultrathin b-axis oriented zeolite membranes. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 507-514. doi: 10.11862/CJIC.20230403
10. [10]
  Lihui Jiang , Wanrong Dong , Hua Yang , Yongqing Xia , Hongjian Peng , Jun Yuan , Xiaoqian Hu , Zihan Zeng , Yingping Zou , Yiming Luo . Study on Extraction of p-Hydroxyacetophenone. University Chemistry, 2024, 39(11): 259-268. doi: 10.12461/PKU.DXHX202402056
11. [11]
  Haiyuan Wang , Xiaoning Jin , Yajing Sun , Zhen Zhang , Wentao Zhao , Yi Li . Practical Exploration of High-Performance Liquid Chromatography Experiment Teaching Reform Empowered by Artificial Intelligence. University Chemistry, 2026, 41(4): 45-51. doi: 10.12461/PKU.DXHX202505076
12. [12]
  Yuanchun Pan , Xinyun Lin , Leyi Yang , Wenya Hu , Dekui Song , Nan Liu . Artificial Intelligence Science Practice: Preparation of Electronic Skin by Chemical Vapor Deposition of Graphene. University Chemistry, 2025, 40(11): 272-280. doi: 10.12461/PKU.DXHX202412052
13. [13]
  Xiaojun Liu , Lang Qin , Yanlei Yu . Dynamic Manipulation of Photonic Bandgaps in Cholesteric Liquid Crystal Microdroplets for Applications. Acta Physico-Chimica Sinica, 2024, 40(5): 2305018-0. doi: 10.3866/PKU.WHXB202305018
14. [14]
  Yifan Xie , Liyun Yao , Ruolin Yang , Yuxing Cai , Yujie Jin , Ning Li . Exploration and Practice of Online and Offline Hybrid Teaching Mode in High-Performance Liquid Chromatography Experiment. University Chemistry, 2025, 40(11): 100-107. doi: 10.12461/PKU.DXHX202412133
15. [15]
  Zhanxiang Liu , Chengshan Yuan , Jie Han , Shuanglian Cai , Qihan Zhang , Lin Wu , Yuan Zheng , Xingwen Sun , Qingwen Liu , Ying Xiong , Guangao Yu , Xin Du , Houjin Li , Jianrong Zhang , Shuyong Zhang . Recommendations for Basic Operations and Standards for Organic Chemical Extraction and Washing Experiments. University Chemistry, 2025, 40(5): 55-65. doi: 10.12461/PKU.DXHX202410039
16. [16]
  Mingyang Men , Jinghua Wu , Gaozhan Liu , Jing Zhang , Nini Zhang , Xiayin Yao . Sulfide Solid Electrolyte Synthesized by Liquid Phase Approach and Application in All-Solid-State Lithium Batteries. Acta Physico-Chimica Sinica, 2025, 41(1): 100004-0. doi: 10.3866/PKU.WHXB202309019
17. [17]
  Gaoyan Chen , Chaoyue Wang , Juanjuan Gao , Junke Wang , Yingxiao Zong , Kin Shing Chan . Heart to Heart: Exploring Cardiac CT. University Chemistry, 2024, 39(9): 146-150. doi: 10.12461/PKU.DXHX202402011
18. [18]
  Jiahao Zhang , Lirong Lin , Zhongning Lin , Shengxiang Ge , Huayun Shi , Hongmin Chen . Exploration and reform of general chemistry experimental course for medical experimental class. University Chemistry, 2026, 41(4): 149-156. doi: 10.12461/PKU.DXHX202503091
19. [19]
  Lingyu Chang , Yanfang Lang , Yuyan Zhu , Jie Wang , Ying Guo , Die Wang , Peng Ding , Yueming Zhou , Zhixiang Gong , Shujuan Liu . Machine Learning-Optimized Microcolumn Ion Exchange Chromatography for Trace Arsenic Determination. University Chemistry, 2026, 41(1): 76-84. doi: 10.12461/PKU.DXHX202506023
20. [20]
  Tengyue ZHANG , Jingjing FENG , Zili LIANG , Jia′nan DAI , Jing MA . Optimization of C-doped BiVO₄ performance for tetracycline degradation using response surface methodology-assisted orthogonal experiments. Chinese Journal of Inorganic Chemistry, 2025, 41(12): 2561-2574. doi: 10.11862/CJIC.20250104

Get Citation

PDF

XML

Metrics

PDF Downloads(0)
Abstract views(863)
HTML views(98)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142