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Citation: HU Weibing, HUANG Meng, FENG Fu, CUI Zhicai, LIU Xinping. Microwave-assisted Michael Additions Between Nitrofluorene and Acrylic Esters[J]. Chinese Journal of Applied Chemistry, ;2013, 30(6): 623-627. doi: 10.3724/SP.J.1095.2013.20368 shu

Microwave-assisted Michael Additions Between Nitrofluorene and Acrylic Esters

HU Weibing ^a, ,
HUANG Meng ^a ,
FENG Fu ^a,b ,
CUI Zhicai ^a ,
LIU Xinping ^a

a. School of Chemistry and Environmental Engineering, Hubei Institute for Nationalities, Enshi 445000, China;
b. Department of Chemistry, Huazhong Normal University, Wuhan 430079, China

Received Date: 27 August 2012
Revised Date: 26 November 2012

Using nitrofluorene and acrylic esters as precursors,a series of Michael addition products with high yields of 79%~87% was obtained under microwave irradiation(500 W) for 4~5 min in the presence of sodium hydroxide. The strcutures of products were characterized by IR,¹H NMR,MS and elemental analysis. The crystal structure of compound 3b was determined by single X-ray diffraction analysis.
- nitrofluorene,
- Michael addition,
- microwave-assisted
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