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正六棱型MoO3-x微米柱光催化剂的制备及性能

唐飞 ,  杜多勤 ,  谭芸妃 ,  秦莉晓

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引用本文: 唐飞, 杜多勤, 谭芸妃, 秦莉晓. 正六棱型MoO3-x微米柱光催化剂的制备及性能[J]. 应用化学, 2021, 38(1): 92-98. doi: 10.19894/j.issn.1000-0518.190335 shu
Citation:  TANG Fei,  DU Duo-Qin,  TAN Yun-Fei,  QIN Li-Xiao. Preparation and Characterization of MoO3-x Hexagonal Microrods as High-Efficiency Photocatalysts[J]. Chinese Journal of Applied Chemistry, 2021, 38(1): 92-98. doi: 10.19894/j.issn.1000-0518.190335 shu

正六棱型MoO3-x微米柱光催化剂的制备及性能

  • 1.

    重庆大学化学化工学院, 重庆 401331;

  • 2.

    重庆斯泰克瑞登梅尔材料技术有限公司, 重庆 401221

    • 通讯作者: 秦莉晓,E-mail:lxqin@cqu.edu.cn
  • 基金项目:

    国家自然科学基金（No.21776025）、中央高校基本科研业务费（Nos.2018CDKYGL0002，2018CDKYHG0028）和重庆市基础研究与前沿技术研究计划（No.CSTC2016JCYJA0474）资助

摘要: 首先采用低温水相合成法制备了正六棱型MoO3微米柱，然后以抗坏血酸为还原剂一步还原法制备了一种表面氧空位可控的MoO3-x光催化材料。MoO3-x具有较窄的禁带宽度和较大的光吸收范围。以罗丹明B为模拟污染物的光催化降解实验表明，随着氧空位的增加，MoO3-x的催化活性明显增加。对于Mo5+摩尔分数为20.1%的MoO2.799样品，降解90%的初始质量浓度为10 mg/L的罗丹明溶液只需要60 min。本研究为高性能半导体光催化材料的制备提供了一种新思路。

English


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  • 收稿日期:  2019-12-16
通讯作者: 陈斌, bchen63@163.com
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