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冷辅助固相微萃取技术在复杂基质样品分析中的应用

李慧敏 ,  周彧琛 ,  肖玉芳 ,  樊静 ,  冯素玲 ,  徐生瑞

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引用本文: 李慧敏, 周彧琛, 肖玉芳, 樊静, 冯素玲, 徐生瑞. 冷辅助固相微萃取技术在复杂基质样品分析中的应用[J]. 分析化学, 2022, 50(9): 1289-1298. doi: 10.19756/j.issn.0253-3820.221157 shu
Citation:  LI Hui-Min,  ZHOU Yu-Chen,  XIAO Yu-Fang,  FAN Jing,  FENG Su-Ling,  XU Sheng-Rui. Application of Cooling-assisted Solid Phase Microextraction in Analysis of Complex Matrix Sample[J]. Chinese Journal of Analytical Chemistry, 2022, 50(9): 1289-1298. doi: 10.19756/j.issn.0253-3820.221157 shu

冷辅助固相微萃取技术在复杂基质样品分析中的应用

  • 1.

    河南师范大学化学化工学院, 新乡 453007;

  • 2.

    湖北省地质实验测试中心, 武汉 430034;

  • 3.

    河南师范大学环境学院, 新乡 453007

    • 通讯作者: 樊静,E-mail:fanjing@htu.edu.cn; 徐生瑞,E-mail:xushengrui@126.com
  • 基金项目:

    国家自然科学基金项目（Nos.21976052，21705017）和河南师范大学青年基金项目（No.20200183）资助。

摘要: 复杂基质样品分析中的绿色样品前处理技术研究一直是分析科学研究的热点之一。顶空固相微萃取技术(HS-SPME)可以实现样品中挥发性有机物的无溶剂萃取分析,但是对于复杂基质样品的萃取难以达到满意效果。冷辅助固相微萃取技术(CA-SPME)可同时实现样品基质加热和涂层冷却,弥补了常规HS-SPME的不足,有效促进了复杂基质样品中挥发性和半挥发性物质的萃取效率,实现了复杂基质样品的无溶剂萃取分析。凭借其独特的优势,CA-SPME为复杂基质样品绿色分析提供了一种新的途径。本文总结了近年来CA-SPME技术的进展,重点讨论了CA-SPME装置的变革以及影响其萃取效率的因素,并介绍了该技术的应用领域,最后对这一技术的研究前景进行了展望,以期为复杂样品分析研究提供参考。

English


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