热提取乳液进样-单颗粒电感耦合等离子体质谱法测定食品包装材料中的纳米银

梁维新 潘佳钏 林晨 郭鹏然

引用本文: 梁维新, 潘佳钏, 林晨, 郭鹏然. 热提取乳液进样-单颗粒电感耦合等离子体质谱法测定食品包装材料中的纳米银[J]. 分析化学, 2021, 49(9): 1572-1579. doi: 10.19756/j.issn.0253-3820.210463 shu
Citation:  LIANG Wei-Xin,  PAN Jia-Chuan,  LIN Chen,  GUO Peng-Ran. Thermal Extraction-emulsion Injection Combining Single Particle-inductively Coupled Plasma-mass Spectrometry for Determination of Sliver Nanoparticles in Food Packaging[J]. Chinese Journal of Analytical Chemistry, 2021, 49(9): 1572-1579. doi: 10.19756/j.issn.0253-3820.210463 shu

热提取乳液进样-单颗粒电感耦合等离子体质谱法测定食品包装材料中的纳米银

    通讯作者: 郭鹏然,E-mail:prguo@fenxi.com.cn
  • 基金项目:

    广东省重点研究领域计划项目(No.2019B020211001)和广东省科学院测试分析研究所自筹科研资金项目(No.202005)资助。

摘要: 建立了热提取乳液进样-单颗粒电感耦合等离子体质谱法测定抗菌包装材料中纳米银颗粒(AgNPs)的方法。采用十氢萘在高温条件下破坏聚乙烯高分子链,提取抗菌包装材料中的AgNPs,通过单颗粒电感耦合等离子质谱法(Single particle-inductively coupled plasma mass spectrometry,SP-ICP-MS)测定了AgNPs的质量/颗粒浓度以及粒径分布,考察了方法的最佳提取温度、提取效率和检出限,并应用于实际样品测定。实验结果表明,热提取过程未对AgNPs的粒径分布和颗粒浓度造成影响,薄膜和袋装两种类型的抗菌包装材料的最佳提取温度为150℃,提取效率分别为94.3%和90.3%,方法的粒径检出限为23 nm。实际样品测试结果显示,4种抗菌包装材料的AgNPs含量在0.038~4.884 μg/g之间,AgNPs占总银的比率在0.69%~3.80%之间,平均粒径在35.5~85.1 nm之间。本方法可快速、准确评价食品包装材料中AgNPs含量及粒度分布。

English


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  • 收稿日期:  2021-04-25
  • 修回日期:  2021-06-21
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