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Citation: Ying-Ying HUANG, Qing-Dou XU, Sheng-Min HU, Xin-Tao WU, Tian-Lu SHENG. Syntheses, Crystal Structures and Different Magnetic Behaviors of Three Cyanide-bridged FeII-MII (M = Fe, Co and Mn) Complexes[J]. Chinese Journal of Structural Chemistry, ;2021, 40(9): 1161-1168. doi: 10.14102/j.cnki.0254–5861.2011–3123 shu

Syntheses, Crystal Structures and Different Magnetic Behaviors of Three Cyanide-bridged FeII-MII (M = Fe, Co and Mn) Complexes

  • a.

    College of Chemistry, Fuzhou University, Fuzhou 350002, China

  • b.

    State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002, China

  • c.

    University of Chinese Academy of Sciences, Beijing 100049, China

  • Corresponding author: Tian-Lu SHENG, tsheng@fjirsm.ac.cn
  • Received Date: 27 January 2021
    Accepted Date: 4 March 2021

    Fund Project: the National Natural Science Foundation of China 21773243the National Natural Science Foundation of China 21973095the Strategic Priority Research Program of the Chinese Academy of Sciences XDB20010200

Figures(4)

  • Three dinuclear cyanide-bridged complexes [FeII(PY5OMe2)CNMII(PY5OMe2)](OTf)3 (M = Fe 1, M = Co 2, M = Mn 3) (PY5OMe2 = 2, 6-bis-((2-pyridyl)methoxymethane)pyridine OTf = CF3SO3-) have been synthesized and characterized. Single-crystal diffraction analyses show these three dinuclear compounds are very similar in structure. The measured ν(CN) results for compounds 1~3 suggest that Mn2+ is electron-poorer than Fe2+ and Co2+. Meanwhile, the temperature dependence of magnetic susceptibilities of complexes 1~3 reveals that in these three complexes, all the cyanide-carbon coordinated Fe(II) is low-spin, and Co(II) for 2 and Mn(II) for 3 are both in a high-spin state through 2~400 K but the cyanide-nitrogen coordinated Fe(II) for complex 1 exhibits spin crossover (SCO) behavior over 300 K and a hysteresis of 36 K in both cooling and heating modes.
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