Preparation and Characterization of ZnMgAl Hydrotalcite Supported BiOI
- Corresponding author: FU Dayou, Fdy888@263.net
Citation:
LI Jiaqi, FU Dayou, YUAN Dong, XU Jing. Preparation and Characterization of ZnMgAl Hydrotalcite Supported BiOI[J]. Chinese Journal of Applied Chemistry,
;2019, 36(1): 83-90.
doi:
10.11944/j.issn.1000-0518.2019.01.180059
Wang L J, Wang L R, Feng Y J. Highly Efficient and Selective Infrared Absorption Material Based on Layered Double Hydroxides for Use in Agricultural Plastic Film[J]. Appl Clay Sci, 2011,53(4):592-597. doi: 10.1016/j.clay.2011.05.008
Wang L J, Xu X Y, Evans D G. Synthesis and Selective IR Absorption Properties of Iminodiacetic-Acid Intercalated MgAl-layered Double Hydroxide[J]. J Solid State Chem, 2010,183(5):1114-1119. doi: 10.1016/j.jssc.2010.03.022
Evants D G, Rct S. Structure Aspects of Layered Double Hydroxide[J]. Struct Bond, 2006,119:1-87.
Zhu H F, Tang P G, Feng Y J. Intercalation of IR Absorber into Layered Double Hydroxides:Preparation, Thermal Stability and Selective IR Absorption[J]. Mater Res Bull, 2012,47(3):532-536. doi: 10.1016/j.materresbull.2011.12.056
Li L D, Yu J J, Hao Z P. Novel Ru-Mg-Al-O Catalyst Derived from Hydrotalcite-Like Compound for NO Storage/Decomposition/Reduction[J]. J Phys Chem C, 2007,111(28):10552-10559. doi: 10.1021/jp0678352
Obalová L, Jirátová K, Kovanda F. Catalytic Decomposition of Nitrous Oxide over Catalysts Prepared from Co/Mg-Mn/Al Hydrotalcite-like Compounds[J]. Appl Catal B-Environ, 2005,60:289-297. doi: 10.1016/j.apcatb.2005.04.002
Shao M, Ning F, Zhao J. Preparation of Fe3O4/SiO2/Layered Double Hydroxide Coreshell Microspheres for Magnetic Separation of Proteins[J]. J Am Chem Soc, 2012,134:1071-1077. doi: 10.1021/ja2086323
Lu X, Wang G, Zhai T. Hydrogenated TiO2 Nanotube Arrays for Supercapacitors[J]. Nano Lett, 2012,12:1690-1696. doi: 10.1021/nl300173j
Yuan D, Zhou L, Fu D Y. Adsorption of Methyl Orange from Aqueous Solutions by Calcined ZnMgAl Hydrotalcite[J]. Appl Phys A-Mater, 2017,123:146-153. doi: 10.1007/s00339-017-0763-2
Xu J Y, Liu J, Li K D. Novel PEPA-Functionalized Graphene Oxide for Fire Safety Enhancement of Polypropylene[J]. Sci Technol Adv Mater, 2015(16):1-11.
Song Y, Wang J, Li Z. Self-assembled Hierarchical Porous Layered Double Hydroxides by Solvothermal Method and Their Application for Capacitors[J]. Micropor Mesopor Mater, 2012,148(1):159-165. doi: 10.1016/j.micromeso.2011.08.013
Zhang L, Zhang X, Shen L. Enhanced High-Current Capacitive Behavior of Graphene/CoAl-layered Double Hydroxide Composites as Electrode Material for Supercapacitors[J]. J Power Sources, 2012,199:395-401. doi: 10.1016/j.jpowsour.2011.10.056
Hou W G, Jin Z L. Synthesis and Characterization of Naproxen Intercalated Zn-Al Layered Double Hydroxides[J]. Colloid Polym Sci, 2007,285(13):1449-1454. doi: 10.1007/s00396-007-1704-y
XUE Yuanming, FAN Lihui, LIU Dongbin. Photocatalytic Degradation of Methyl Orange on ZnCr Layered Double Hydroxides[J]. J Shenyang Univ Chem Tech, 2015,29(3):233-237. doi: 10.3969/j.issn.2095-2198.2015.03.009
WANG Lina. Prepapation and Properties of Go/BiOI Composite Visible-Light Photocatalytic Materials[D]. Harbin: Harbin Normal University, 2013(in Chinese).
Chen L, Huang R, Xiong M. Room-Temperature Synthesis of Flower-Like BiOX(X=Cl, Br, I) Hierarchical Structures and Their Visible-Light Photocatalytic Activity[J]. Inorg Chem, 2013,52(19):11118-11125. doi: 10.1021/ic401349j
Liu Q C, Ma D K, Hu Y Y. Various Bismuth Oxyiodide Hierarchical Architectures:Alcohothermal-Controlled Synthesis, Photocatalytic Activities, and Adsorption Capabilities for Phosphate in Water[J]. ACS Appl Mater Interfaces, 2013,5(22):11927-11934. doi: 10.1021/am4036702
WANG Na, ZHONG Jianchu, WANG Hongzhi. Preparation, Characterization and Application of Calcium and Aluminum Layered Double Hydroxides Intercalated by Boric Acid Radical[J]. Inorg Chem Ind, 2016,48(1):25-27.
WANG Ruirui. Studies on Synthesis and Properties of Layered Double Hydroxides Intercalated with Drugs[D]. Harbin: Harbin Engineering University, 2012(in Chinese).
Wang J T, Xu F. Preparation of EDTA Pillared MgZnAl LDHs and Its Adsorption of Pb(Ⅱ)[J]. Chem Res Appl, 2014,26(4):581-585.
Han X G, He H Z, Kuang Q. Controlling Morphologies and Tuning the Related Properties of Nano/Microstructured ZnO Crystallites[J]. J Phys Chem C, 2009,113(2):584-589.
Yaping ZHANG , Tongchen WU , Yun ZHENG , Bizhou LIN . Z-scheme heterojunction β-Bi2O3 pillared CoAl layered double hydroxide nanohybrid: Fabrication and photocatalytic degradation property. Chinese Journal of Inorganic Chemistry, 2025, 41(3): 531-539. doi: 10.11862/CJIC.20240256
Fangxuan Liu , Ziyan Liu , Guowei Zhou , Tingting Gao , Wenyu Liu , Bin Sun . 中空结构光催化剂. Acta Physico-Chimica Sinica, 2025, 41(7): 100071-0. doi: 10.1016/j.actphy.2025.100071
Xian-Wei Lv , Xinyuan Ding , Jiaxing Gong , Xuhuan Yan , Dayong Huang , Jianxin Geng , Zhong-Yong Yuan . Research progress on orbital hybridization in photocatalysis and electrocatalysis. Acta Physico-Chimica Sinica, 2026, 42(2): 100151-0. doi: 10.1016/j.actphy.2025.100151
Xianghai Song , Xiaoying Liu , Zhixiang Ren , Xiang Liu , Mei Wang , Yuanfeng Wu , Weiqiang Zhou , Zhi Zhu , Pengwei Huo . Insights into the greatly improved catalytic performance of N-doped BiOBr for CO2 photoreduction. Acta Physico-Chimica Sinica, 2025, 41(6): 100055-0. doi: 10.1016/j.actphy.2025.100055
Qiang ZHAO , Zhinan GUO , Shuying LI , Junli WANG , Zuopeng LI , Zhifang JIA , Kewei WANG , Yong GUO . Cu2O/Bi2MoO6 Z-type heterojunction: Construction and photocatalytic degradation properties. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 885-894. doi: 10.11862/CJIC.20230435
Aoyun Meng , Zhenhua Li , Guoyuan Xiong , Zhen Li , Jinfeng Zhang . S-scheme heterojunction Al6Si2O13/BiOBr with enhanced charge transfer effect for efficient and stable photocatalytic degradation of triazophos and dichlorvos pesticides. Acta Physico-Chimica Sinica, 2026, 42(5): 100186-0. doi: 10.1016/j.actphy.2025.100186
Tengyue ZHANG , Jingjing FENG , Zili LIANG , Jia′nan DAI , Jing MA . Optimization of C-doped BiVO4 performance for tetracycline degradation using response surface methodology-assisted orthogonal experiments. Chinese Journal of Inorganic Chemistry, 2025, 41(12): 2561-2574. doi: 10.11862/CJIC.20250104
Zhiquan Zhang , Baker Rhimi , Zheyang Liu , Min Zhou , Guowei Deng , Wei Wei , Liang Mao , Huaming Li , Zhifeng Jiang . Insights into the Development of Copper-Based Photocatalysts for CO2 Conversion. Acta Physico-Chimica Sinica, 2024, 40(12): 2406029-0. doi: 10.3866/PKU.WHXB202406029
Jiali Lei , Juan Wang , Wenhui Zhang , Guohong Wang , Zihui Liang , Jinmao Li . TiO2/CdIn2S4 S-scheme heterojunction photocatalyst promotes photocatalytic hydrogen evolution coupled vanillyl alcohol oxidation. Acta Physico-Chimica Sinica, 2025, 41(12): 100174-0. doi: 10.1016/j.actphy.2025.100174
Jingping Li , Suding Yan , Jiaxi Wu , Qiang Cheng , Kai Wang . Improving hydrogen peroxide photosynthesis over inorganic/organic S-scheme photocatalyst with LiFePO4. Acta Physico-Chimica Sinica, 2025, 41(9): 100104-0. doi: 10.1016/j.actphy.2025.100104
Ping ZHANG , Chenchen ZHAO , Xiaoyun CUI , Bing XIE , Yihan LIU , Haiyu LIN , Jiale ZHANG , Yu'nan CHEN . Preparation and adsorption-photocatalytic performance of ZnAl@layered double oxides. Chinese Journal of Inorganic Chemistry, 2024, 40(10): 1965-1974. doi: 10.11862/CJIC.20240014
Yi Yang , Xin Zhou , Miaoli Gu , Bei Cheng , Zhen Wu , Jianjun Zhang . Femtosecond transient absorption spectroscopy investigation on ultrafast electron transfer in S-scheme ZnO/CdIn2S4 photocatalyst for H2O2 production and benzylamine oxidation. Acta Physico-Chimica Sinica, 2025, 41(6): 100064-0. doi: 10.1016/j.actphy.2025.100064
Yuchen Zhou , Huanmin Liu , Hongxing Li , Xinyu Song , Yonghua Tang , Peng Zhou . Designing thermodynamically stable noble metal single-atom photocatalysts for highly efficient non-oxidative conversion of ethanol into high-purity hydrogen and value-added acetaldehyde. Acta Physico-Chimica Sinica, 2025, 41(6): 100067-0. doi: 10.1016/j.actphy.2025.100067
Qinhui Guan , Yuhao Guo , Na Li , Jing Li , Tingjiang Yan . Molecular sieve-mediated indium oxide catalysts for enhancing photocatalytic CO2 hydrogenation. Acta Physico-Chimica Sinica, 2025, 41(11): 100133-0. doi: 10.1016/j.actphy.2025.100133
Qingqing SHEN , Xiangbowen DU , Kaicheng QIAN , Zhikang JIN , Zheng FANG , Tong WEI , Renhong LI . Self-supporting Cu/α-FeOOH/foam nickel composite catalyst for efficient hydrogen production by coupling methanol oxidation and water electrolysis. Chinese Journal of Inorganic Chemistry, 2024, 40(10): 1953-1964. doi: 10.11862/CJIC.20240028
Huiwei Ding , Bo Peng , Zhihao Wang , Qiaofeng Han . Advances in Metal or Nonmetal Modification of Bismuth-Based Photocatalysts. Acta Physico-Chimica Sinica, 2024, 40(4): 2305048-0. doi: 10.3866/PKU.WHXB202305048
Yushan Cai , Fang-Xing Xiao . Revisiting MXenes-based Photocatalysis Landscape: Progress, Challenges, and Future Perspectives. Acta Physico-Chimica Sinica, 2024, 40(8): 2306048-0. doi: 10.3866/PKU.WHXB202306048
Juntao Yan , Liang Wei . 2D S-Scheme Heterojunction Photocatalyst. Acta Physico-Chimica Sinica, 2024, 40(10): 2312024-0. doi: 10.3866/PKU.WHXB202312024
Yuanyin Cui , Jinfeng Zhang , Hailiang Chu , Lixian Sun , Kai Dai . Rational Design of Bismuth Based Photocatalysts for Solar Energy Conversion. Acta Physico-Chimica Sinica, 2024, 40(12): 2405016-0. doi: 10.3866/PKU.WHXB202405016
Yu Liu , Pengfei Li , Yize Liu , Zaicheng Sun . Recent advances in carbon dots as a single photocatalyst. Acta Physico-Chimica Sinica, 2026, 42(2): 100167-0. doi: 10.1016/j.actphy.2025.100167
a.ZnMgAl-HTLCs; b.BiOI/ZnMgAl-HTLCs; c.BiOI
A.ZnMgAl-HTLCs; B.BiOI; C.BiOI/ZnMgAl-HTLCs
w(BiOI)/%:A.30; B.40; C.50; D.60
w(BiOI)/%:a.60; b.50; c.40; d.30
A.Adding ZnMgAL-HTLCs before pH adjustment; B.Adding ZnMgAL-HTLCs after pH adjustment
A.80 ℃; B.100 ℃; C.120 ℃; D.140 ℃
a.80 ℃; b.100 ℃; c.120 ℃; d.140 ℃
A.8 h; B.12 h; C.15 h; D.24 h
a.8 h; b.12 h; c.15 h; d.24 h
a.DTG curve; b.TG curve
a.DTG curve; b.TG curve